世界科学技术-中医药现代化
世界科學技術-中醫藥現代化
세계과학기술-중의약현대화
WORLD SCIENCE AND TECHNOLOGY-MODERNIZATION OF TRADITIONAL CHINESE MEDICINE
2014年
11期
2371-2379
,共9页
陈罡%黄亮%李文佳%詹泽苹%辛立波%艾中%钱正明%刘国柱
陳罡%黃亮%李文佳%詹澤蘋%辛立波%艾中%錢正明%劉國柱
진강%황량%리문가%첨택평%신립파%애중%전정명%류국주
冬虫夏草%核磁指纹图谱%水提物%醇提物
鼕蟲夏草%覈磁指紋圖譜%水提物%醇提物
동충하초%핵자지문도보%수제물%순제물
Cordyceps sinensis%NMR fingerprint%water extract%methanol extract
目前冬虫夏草市场伪品泛滥,鉴别困难。本文采用核磁共振技术对3个不同产地的21批野生冬虫夏草、30批冬虫夏草野生抚育品和4种冬虫夏草伪品的水提物及醇提物进行了测定,比较分析之后确定了9组特征峰作为量化标准,建立了冬虫夏草的核磁特征指纹图谱。对野生冬虫夏草、冬虫夏草野生抚育品和冬虫夏草伪品的核磁特征指纹图谱进行比较分析发现,野生冬虫夏草和冬虫夏草野生抚育品具有高度的相似性,4种冬虫夏草伪品的核磁特征图谱与野生冬虫夏草及冬虫夏草野生抚育品的核磁指纹图谱均存在不同程度的差异。比对结果也显示,冬虫夏草的核磁指纹图谱具有很强的特征性和专属性。野生冬虫夏草与冬虫夏草野生抚育品核磁指纹图谱具有良好的一致性,表明两种冬虫夏草的化学成分基本相同。
目前鼕蟲夏草市場偽品汎濫,鑒彆睏難。本文採用覈磁共振技術對3箇不同產地的21批野生鼕蟲夏草、30批鼕蟲夏草野生撫育品和4種鼕蟲夏草偽品的水提物及醇提物進行瞭測定,比較分析之後確定瞭9組特徵峰作為量化標準,建立瞭鼕蟲夏草的覈磁特徵指紋圖譜。對野生鼕蟲夏草、鼕蟲夏草野生撫育品和鼕蟲夏草偽品的覈磁特徵指紋圖譜進行比較分析髮現,野生鼕蟲夏草和鼕蟲夏草野生撫育品具有高度的相似性,4種鼕蟲夏草偽品的覈磁特徵圖譜與野生鼕蟲夏草及鼕蟲夏草野生撫育品的覈磁指紋圖譜均存在不同程度的差異。比對結果也顯示,鼕蟲夏草的覈磁指紋圖譜具有很彊的特徵性和專屬性。野生鼕蟲夏草與鼕蟲夏草野生撫育品覈磁指紋圖譜具有良好的一緻性,錶明兩種鼕蟲夏草的化學成分基本相同。
목전동충하초시장위품범람,감별곤난。본문채용핵자공진기술대3개불동산지적21비야생동충하초、30비동충하초야생무육품화4충동충하초위품적수제물급순제물진행료측정,비교분석지후학정료9조특정봉작위양화표준,건립료동충하초적핵자특정지문도보。대야생동충하초、동충하초야생무육품화동충하초위품적핵자특정지문도보진행비교분석발현,야생동충하초화동충하초야생무육품구유고도적상사성,4충동충하초위품적핵자특정도보여야생동충하초급동충하초야생무육품적핵자지문도보균존재불동정도적차이。비대결과야현시,동충하초적핵자지문도보구유흔강적특정성화전속성。야생동충하초여동충하초야생무육품핵자지문도보구유량호적일치성,표명량충동충하초적화학성분기본상동。
The inundation of Cordyceps sinensis counterfeits in the market makes it difficult to identify. In this study, 21 batches of wild C. sinensis from 3 different regions, 30 batches of naturally cultured C. sinensis and 4 kinds of counterfeits extracted by methanol and water were analyzed using NMR technology. 9 characteristic peaks were defined as quantitative criterion after comparison, and NMR fingerprints of C. sinensis were established. According to the result it is highly similar between naturally cultured C. sinensis and wild ones by comparing their NMR fingerprints. However, NMR spectra of four kinds of adulterants showed differences with C. sinensis. The result also showed that NMR fingerprint of C. sinensis are highly characteristic and specific. The NMR characteristic fingerprint of wild C. sinensis was consistent with the naturally cultured C. sinensis, and it indicated that the chemical constituents of wild C. sinensis and naturally cultured C. sinensis are nearly the same.