CAJ | 학술논문

目的：对仙龙解毒饮的薄层鉴别和含量测定进行研究。方法采用TLC对处方中麦冬、甘草进行定性鉴别；采用UV-HPLC测定甘草中甘草苷含量。结果薄层色谱中均检出麦冬、甘草，斑点清晰，阴性均无干扰，专属性强。甘草苷在11.0～109.6μg· mL－1范围内呈现良好的线性关系（r2＝0.9996），平均加样回收率为101.2％（RSD＝1.55％）。结论本实验建立的方法简便、准确、重现性好，可作为仙龙解毒饮的质量控制。
목적：대선룡해독음적박층감별화함량측정진행연구。방법채용TLC대처방중맥동、감초진행정성감별；채용UV-HPLC측정감초중감초감함량。결과박층색보중균검출맥동、감초，반점청석，음성균무간우，전속성강。감초감재11.0～109.6μg· mL－1범위내정현량호적선성관계（r2＝0.9996），평균가양회수솔위101.2％（RSD＝1.55％）。결론본실험건립적방법간편、준학、중현성호，가작위선룡해독음적질량공제。
OBJECTIVE To study the TLC Identification and Content Determination of Xianlong Jiedu Yin.METHODS TLC method was used to identify radix ophiopogonis and liquorice.The content of liquritin was determined by UV-HPLC.RESULTS The spots on TLC plates were clear without interference in the blank refer-ence.The response of liquritin was linear in the ranges of 11.0~109.6μg· mL-1(r2 =0.9996),the average recov-ery was 101.2%,RSD=1.55%.CONCLUSION The method is simple,accurate,reproducible and can be used for the quality control of Xianlong Jiedu Yin.