CAJ | 학술논문

针对隔壁精馏塔节能工艺，提供了一套完整的设计优化方法。首先基于 Fenske-Underwood-Gilliland-Kirkbride 方程建立了完整的简捷设计方法，得到了隔壁精馏塔塔实际理论板数、适宜的进料位置、侧线采出位置及回流比等参数。然后在简捷计算的基础之上，选用 Multifrac 模型对隔壁塔进行了严格计算模拟，同时利用 Aspen Plus 进行单因素优化分析得到最优设计参数。最后利用响应面优化法(RSM)中的箱线图设计(BBD)方法对隔壁精馏塔设计参数进行了实验设计，在验证模型有效的基础上运用Design-Expert软件进行数据处理，预测出了最优设计参数，并将预测值进行实验验证，将验证结果与单因素优化结果进行对比，结果表明响应面优化法得到的最优设计参数使隔壁塔的能耗较低、纯度较高。
침대격벽정류탑절능공예，제공료일투완정적설계우화방법。수선기우 Fenske-Underwood-Gilliland-Kirkbride 방정건립료완정적간첩설계방법，득도료격벽정류탑탑실제이론판수、괄의적진료위치、측선채출위치급회류비등삼수。연후재간첩계산적기출지상，선용 Multifrac 모형대격벽탑진행료엄격계산모의，동시이용 Aspen Plus 진행단인소우화분석득도최우설계삼수。최후이용향응면우화법(RSM)중적상선도설계(BBD)방법대격벽정류탑설계삼수진행료실험설계，재험증모형유효적기출상운용Design-Expert연건진행수거처리，예측출료최우설계삼수，병장예측치진행실험험증，장험증결과여단인소우화결과진행대비，결과표명향응면우화법득도적최우설계삼수사격벽탑적능모교저、순도교고。
A set of comprehensive methods was proposed for the design and optimization of divided wall col-umn(DWC). A short-cut design method based on Fenske-Underwood-Gilliland-Kirkbride equations for DWC was used to get initial values of design parameters of theoretical stages,feed stage,side-product stage,reflux ratio and so on. With the initial values of all parameters from short-cut design,rigorous simulation of DWC was carried out using Multifrac model. The optimization result was obtained through single-factor experiment using Aspen Plus. In the last stage,Box-Behnken design(BBD)under response surface methodology(RSM)was used for the optimization of DWC and to evaluate the effects of parameters and their interactions on energy efficiency and product purity. Design-Expert software was used to tackle experiment data and predict optimization result based on significant model. Com-paring the optimization result of single-factor experiment and RSM,we found that RSM could render more optimized result in respect of energy saving and high purity.