西南师范大学学报(自然科学版)
西南師範大學學報(自然科學版)
서남사범대학학보(자연과학판)
JOURNAL OF SOUTHWEST CHINA NORMAL UNIVERSITY
2014年
12期
65-68
,共4页
田金凤%尚远宏%王深红%汪宏锦%杨艳涵%刘圆
田金鳳%尚遠宏%王深紅%汪宏錦%楊豔涵%劉圓
전금봉%상원굉%왕심홍%왕굉금%양염함%류원
β 环糊精%挥发油%水蒸气蒸馏法%陈皮%白术
β 環糊精%揮髮油%水蒸氣蒸餾法%陳皮%白術
β 배호정%휘발유%수증기증류법%진피%백술
essential oil,β-cyclodextrin%steam distillation method%Citri reticulatae pericarpium,A trac-tylodis macrocephalae Koidiz
确定陈皮、白术挥发油提取及其包合物制备最佳工艺.方法:水蒸气蒸馏提取挥发油和饱和水溶液法制备包合物,并用正交试验法,对挥发油提取与β环糊精的包合进行3因素3水平考察.结果:最佳提取工艺A2 B2 C3,即陈皮、白术粉碎成过50目筛的粉末,加10倍水量,提取5 h;最佳包合工艺A3 B2 C1,即用挥发油与β‐CD投料比为1∶6,50℃搅拌包合5 h ,包合率为81.90%.结论:提取和包合工艺简单、易行、成本较低.
確定陳皮、白術揮髮油提取及其包閤物製備最佳工藝.方法:水蒸氣蒸餾提取揮髮油和飽和水溶液法製備包閤物,併用正交試驗法,對揮髮油提取與β環糊精的包閤進行3因素3水平攷察.結果:最佳提取工藝A2 B2 C3,即陳皮、白術粉碎成過50目篩的粉末,加10倍水量,提取5 h;最佳包閤工藝A3 B2 C1,即用揮髮油與β‐CD投料比為1∶6,50℃攪拌包閤5 h ,包閤率為81.90%.結論:提取和包閤工藝簡單、易行、成本較低.
학정진피、백술휘발유제취급기포합물제비최가공예.방법:수증기증류제취휘발유화포화수용액법제비포합물,병용정교시험법,대휘발유제취여β배호정적포합진행3인소3수평고찰.결과:최가제취공예A2 B2 C3,즉진피、백술분쇄성과50목사적분말,가10배수량,제취5 h;최가포합공예A3 B2 C1,즉용휘발유여β‐CD투료비위1∶6,50℃교반포합5 h ,포합솔위81.90%.결론:제취화포합공예간단、역행、성본교저.
The paper is related to the investigation of the optimum extraction and inclusion condition of es‐sential oil in A tractylodis macrocephalae Koidiz .and Citri reticulatae pericarpium .The technique of ex‐traction and inclusion are steam distillation method and saturated water solution ,respectively .3 factors and 3 levels orthogonal design have been adopted to explore the optimum conditions .Extreme difference a‐nalysis and variance analysis has been used for data processing .Conditions for the extraction and inclusion of essential oil have been studied .Best extraction process of essential oil in A tractylodis macrocephalae Koidiz .and Citri reticulatae pericarpium is A2 B2 C3 :raw drug materials are boiled 5 hours by addition of 10 times of water to the middle powder (50 mesh screen) of A tractylodis macrocephalae Koidiz .and Citri reticulatae pericarpium .Moreover ,its best inclusion process is A3B2C1 :the proportion of essential oil andβ‐cyclodextrin is 1 :6 ,inclusion time is 1h at the temperature of 50 ℃ ,inclusion rate is 81 .90 % .It is concluded that the extraction and inclusion process of essential oil from A tractylodis macrocephalae Koidiz .and Citri reticulatae pericarpium are simple ,available and economic .