广东石油化工学院学报
廣東石油化工學院學報
엄동석유화공학원학보
JOURNAL OF MAOMING COLLEGE
2014年
6期
1-5
,共5页
弹丸焦%微观形貌%偏光显微%扫描电镜
彈汍焦%微觀形貌%偏光顯微%掃描電鏡
탄환초%미관형모%편광현미%소묘전경
Shot coke%Microtopography%Hardness%Polarizing microscope%SEM
由于渣油劣质化和苛刻的操作条件,在生成石油焦的过程中夹杂出现弹丸焦的几率越来越大。为了更加准确地判断石油焦的种类及理化性质差异,选取典型针状焦、海绵焦、弹丸焦为研究对象,采用电镜扫描、偏光显微等方法进行特性表征,所得图像比以往文献的更加清晰可辨。微观形貌分析较外观形态等宏观性质的分析更能准确全面反映弹丸焦与其它石油焦的特性差异。将扫描电镜、偏光显微镜图片结合起来可以较为清晰地区分各种焦炭的微观外貌差异,为深入研究焦炭(特别是弹丸焦)的微观性质及生焦历程提供了分析判断的参考依据。
由于渣油劣質化和苛刻的操作條件,在生成石油焦的過程中夾雜齣現彈汍焦的幾率越來越大。為瞭更加準確地判斷石油焦的種類及理化性質差異,選取典型針狀焦、海綿焦、彈汍焦為研究對象,採用電鏡掃描、偏光顯微等方法進行特性錶徵,所得圖像比以往文獻的更加清晰可辨。微觀形貌分析較外觀形態等宏觀性質的分析更能準確全麵反映彈汍焦與其它石油焦的特性差異。將掃描電鏡、偏光顯微鏡圖片結閤起來可以較為清晰地區分各種焦炭的微觀外貌差異,為深入研究焦炭(特彆是彈汍焦)的微觀性質及生焦歷程提供瞭分析判斷的參攷依據。
유우사유렬질화화가각적조작조건,재생성석유초적과정중협잡출현탄환초적궤솔월래월대。위료경가준학지판단석유초적충류급이화성질차이,선취전형침상초、해면초、탄환초위연구대상,채용전경소묘、편광현미등방법진행특성표정,소득도상비이왕문헌적경가청석가변。미관형모분석교외관형태등굉관성질적분석경능준학전면반영탄환초여기타석유초적특성차이。장소묘전경、편광현미경도편결합기래가이교위청석지구분각충초탄적미관외모차이,위심입연구초탄(특별시탄환초)적미관성질급생초역정제공료분석판단적삼고의거。
Due to the inferior residue and harsh operating conditions ,shot cokes appear frequently in the process of generating petroleum coke .In order to more accurately determine the type of petroleum coke and its physical and chemical properties ,the types of petroleum coke are reviewed ,and the differences between the physical and chemical properties are analyzed .Typical needle coke (Tested in Jinzhou petrochemical laboratory ) ,Sponge coke (Saudi Arabia reducing slag ,) and the shot coke (Solusy ,Castilla ,Basra mix oil reducing slag ) are analyzed and distinguished by scanning elect microtopography (SEM ) and Polarizing optical microscope (POM ) .Analysis of the macro-scopic properties can more clearly and comprehensively reflect the needle coke and other projectile focal features of the product than appear-ance form analysis .The method combines SEM and POM ,and it can more clearly distinguish the various coke microstructure ,providing analysis and judgment reference for in-depth studying on the microstructure and coking process of coke(especially the shot coke) .