CAJ | 학술논문

以氯化铜为铜源，甲醇、乙醇、异丙醇等为溶剂和还原剂，采用溶剂热法制备纳米氯化亚铜，探讨了温度、时间、还原剂等条件对所得氯化亚铜的形貌、粒径大小、物相组成的影响。结果表明，以乙醇、异丙醇为溶剂，在120~180℃反应24~48 h，CuCl纳米颗粒可在2~50 nm范围内有效调控。
이록화동위동원，갑순、을순、이병순등위용제화환원제，채용용제열법제비납미록화아동，탐토료온도、시간、환원제등조건대소득록화아동적형모、립경대소、물상조성적영향。결과표명，이을순、이병순위용제，재120~180℃반응24~48 h，CuCl납미과립가재2~50 nm범위내유효조공。
A solvothermal method has been developed to prepare cuprous chloride nanoparticles by reduc-ing copper chloride with methanol,ethanol and isopropanol as reducing agents and solvents,and the influ-ences of different reaction conditions such as temperatures,time and reducing agents upon the morpholo-gy,particle size and phase composition of the cuprous chloride were studied. The result showed that with ethanol and isopropanol as solvent,react 24~48 h at 120~180℃. The size of CuCl nanoparticles can be controlled in the range of 2~50 nm effectively.