食品安全质量检测学报
食品安全質量檢測學報
식품안전질량검측학보
FOOD SAFETY AND QUALITY DETECTION TECHNOLOGY
2014年
12期
3988-3991
,共4页
张宏康%王中瑗%林奕楠%麦蕴诗
張宏康%王中瑗%林奕楠%麥蘊詩
장굉강%왕중원%림혁남%맥온시
流动注射分析法%编结反应器%电感耦合等离子体质谱
流動註射分析法%編結反應器%電感耦閤等離子體質譜
류동주사분석법%편결반응기%전감우합등리자체질보
flow injection%knotted reactor%inductively coupled plasma mass spectrometry
电感耦合等离子体质谱技术(ICP-MS)是一种有效用于元素检测的现代分析方法。文中简述了ICP-MS和流动注射分析法(FI)的基本原理; FI做为一种样品引入方式和多功能的在线样品处理手段以其特有的优点越来越广泛的在ICP-MS分析中得到应用。FI使ICP-MS 对高盐溶液承受力提高,使在小稀释因数下将样品溶液引入ICP-MS成为可能,从而可以降低检出限; FI-ICP-MS对有机溶剂有较高的承受力解决了ICP-MS分析含有机物质溶液时的一些问题。本文综述了 FI-ICP-MS 联用技术在分析环境、生物样品、药品、食品等样品中的研究进展以及微流动注射、芯片纳流动注射和等离子体质谱的联用进展。并指出随着我国国力的增强,经济的发展将会使ICP-MS越来越普及, FI-ICP-MS的联用技术研究越来越受到关注,其应用范围也将会大大拓宽。
電感耦閤等離子體質譜技術(ICP-MS)是一種有效用于元素檢測的現代分析方法。文中簡述瞭ICP-MS和流動註射分析法(FI)的基本原理; FI做為一種樣品引入方式和多功能的在線樣品處理手段以其特有的優點越來越廣汎的在ICP-MS分析中得到應用。FI使ICP-MS 對高鹽溶液承受力提高,使在小稀釋因數下將樣品溶液引入ICP-MS成為可能,從而可以降低檢齣限; FI-ICP-MS對有機溶劑有較高的承受力解決瞭ICP-MS分析含有機物質溶液時的一些問題。本文綜述瞭 FI-ICP-MS 聯用技術在分析環境、生物樣品、藥品、食品等樣品中的研究進展以及微流動註射、芯片納流動註射和等離子體質譜的聯用進展。併指齣隨著我國國力的增彊,經濟的髮展將會使ICP-MS越來越普及, FI-ICP-MS的聯用技術研究越來越受到關註,其應用範圍也將會大大拓寬。
전감우합등리자체질보기술(ICP-MS)시일충유효용우원소검측적현대분석방법。문중간술료ICP-MS화류동주사분석법(FI)적기본원리; FI주위일충양품인입방식화다공능적재선양품처리수단이기특유적우점월래월엄범적재ICP-MS분석중득도응용。FI사ICP-MS 대고염용액승수력제고,사재소희석인수하장양품용액인입ICP-MS성위가능,종이가이강저검출한; FI-ICP-MS대유궤용제유교고적승수력해결료ICP-MS분석함유궤물질용액시적일사문제。본문종술료 FI-ICP-MS 련용기술재분석배경、생물양품、약품、식품등양품중적연구진전이급미류동주사、심편납류동주사화등리자체질보적련용진전。병지출수착아국국력적증강,경제적발전장회사ICP-MS월래월보급, FI-ICP-MS적련용기술연구월래월수도관주,기응용범위야장회대대탁관。
Inductively coupled plasma mass spectrometry (ICP-MS) is one of the modern analytical methods for the detection of elements. In this paper, the basic principles of ICP-MS and flow injection (FI) were introduced. As a sample injection method and on-line sample treatment method, FI is widely combined with ICP-MS analysis with its unique merit. Combined with FI, the enduring capacity of ICP-MS to high salt solution is improved and decreases the detection limit, which makes it possible for the injection of samples into ICP-MS with small dilution factor. At the same time, the high enduring capacity of FI-ICP-MS to organic solvent can resolve the problems caused by the organic material solution. The development of FI-ICP-MS applied in environmental samples, biological samples and food samples were reviewed briefly. The development of microchip-based nanoflow injection, chip-based microflow injection and inductively coupled plasma mass spectrometry was also discussed. It indicates that the FI-ICP-MS will be applied and studied more and more widely in China with its rising economy and comprehensive national strength.