中国民族民间医药
中國民族民間醫藥
중국민족민간의약
CHINESE JOURNAL OF ETHNOMEDICINE AND ETHNOPHARMACY
2014年
24期
19-20,22
,共3页
风寒感冒颗粒%HPLC%TLC%质量标准
風寒感冒顆粒%HPLC%TLC%質量標準
풍한감모과립%HPLC%TLC%질량표준
Fenghan Ganmao Granules%HPLC puerarin%TLC%quality standard
目的：建立风寒感冒颗粒的质量控制标准。方法：采用HPLC测定葛根素的含量，薄层色谱法TLC鉴别方中的葛根、麻黄及陈皮。结果：定量方法简单、准确。葛根素在0．0230～0．5750μg浓度范围内呈良好的线性关系，线性方程：Y＝4428．2X－6．9577，R2＝1；葛根素平均回收率98．76％，RSD为1．5％（n＝6）。TLC鉴别专属性强，无干扰。结论：本质量标准可有效的控制风寒感冒颗粒的质量。
目的：建立風寒感冒顆粒的質量控製標準。方法：採用HPLC測定葛根素的含量，薄層色譜法TLC鑒彆方中的葛根、痳黃及陳皮。結果：定量方法簡單、準確。葛根素在0．0230～0．5750μg濃度範圍內呈良好的線性關繫，線性方程：Y＝4428．2X－6．9577，R2＝1；葛根素平均迴收率98．76％，RSD為1．5％（n＝6）。TLC鑒彆專屬性彊，無榦擾。結論：本質量標準可有效的控製風寒感冒顆粒的質量。
목적：건립풍한감모과립적질량공제표준。방법：채용HPLC측정갈근소적함량，박층색보법TLC감별방중적갈근、마황급진피。결과：정량방법간단、준학。갈근소재0．0230～0．5750μg농도범위내정량호적선성관계，선성방정：Y＝4428．2X－6．9577，R2＝1；갈근소평균회수솔98．76％，RSD위1．5％（n＝6）。TLC감별전속성강，무간우。결론：본질량표준가유효적공제풍한감모과립적질량。
Objective To establish the quality standard for Fenghan Ganmao Granules.Method The contents of puerarin were de-termined by HPLC.TLC was used to identify Radix Puerariae,Pericarpium Citri reticulatae Blanco and Ephedra sinica Stapf.Re-sults The linear range of puerarin was 0. 0230~0. 5750μg,y =4428. 2x-6. 9577,R2 =1.The average recovery was 98.76% , RSD 1.5% (n=6).The compounds were identified by TLC .Conclusion The methods are simple.The result is accurate ,the reproducibility is good.There mothods can be used as the quality control of Fenghanganmao Granules.
