中国中医药现代远程教育
中國中醫藥現代遠程教育
중국중의약현대원정교육
CHINESE MEDICINE MODERN DISTANCE EDUCATION OF CHINA
2014年
22期
111-113
,共3页
黄连紫草凝胶%质量标准%高效液相色谱%薄层色谱
黃連紫草凝膠%質量標準%高效液相色譜%薄層色譜
황련자초응효%질량표준%고효액상색보%박층색보
Rhizoma coptidis radix arnebiae seu lithospermi gel%quality standards%HPLC%thin layer chromatography
目的：建立黄连紫草凝胶的质量标准。方法采用TLC鉴别黄连紫草凝胶中的黄连、地黄、当归、紫草、黄柏；采用HPLC对制剂中的盐酸小檗碱进行含量测定。结果盐酸小檗碱在7.64~38.2μg·mL-1范围内线性良好，平均回收率100.38%， RSD3.79%。结论该方法简单易操作，结果准确可靠，重复性好，可作为黄连紫草凝胶的质量控制标准。
目的：建立黃連紫草凝膠的質量標準。方法採用TLC鑒彆黃連紫草凝膠中的黃連、地黃、噹歸、紫草、黃柏；採用HPLC對製劑中的鹽痠小檗堿進行含量測定。結果鹽痠小檗堿在7.64~38.2μg·mL-1範圍內線性良好，平均迴收率100.38%， RSD3.79%。結論該方法簡單易操作，結果準確可靠，重複性好，可作為黃連紫草凝膠的質量控製標準。
목적：건립황련자초응효적질량표준。방법채용TLC감별황련자초응효중적황련、지황、당귀、자초、황백；채용HPLC대제제중적염산소벽감진행함량측정。결과염산소벽감재7.64~38.2μg·mL-1범위내선성량호，평균회수솔100.38%， RSD3.79%。결론해방법간단역조작，결과준학가고，중복성호，가작위황련자초응효적질량공제표준。
Objective Establish the quality standards of rhizoma coptidis radix arnebiae seu lithospermi gel. Methods The TLC identifica-tion of rhizoma coptidis in rhizoma coptidis, radix rehmanniae, radix arnebiae seu lithospermi gel angelica, radix arnebiae seu lithospermi, cortex phellodendri; Content of the preparation of berberine hydrochloride by HPLC determination. Results Berberine hydrochloride in 7.64~38.2μg·mL-1 within the scope of linear is good, the average recovery of 100.38%, RSD3.79%. Conclusion The method is simple and easy to operate, reliable results are accurate and good repeatability can be used as the quality control of rhizoma coptidis radix arnebiae seu lithospermi gel.
