分析测试技术与仪器
分析測試技術與儀器
분석측시기술여의기
ANALYSIS AND TESTING TECHNOLOGY AND INSTRUMENTS
2014年
4期
204-209
,共6页
周静%项超力%刘亚辉%曹代利%陈铃%唐劲松%费长书
週靜%項超力%劉亞輝%曹代利%陳鈴%唐勁鬆%費長書
주정%항초력%류아휘%조대리%진령%당경송%비장서
裂解气相色谱质谱法%氨纶%油剂
裂解氣相色譜質譜法%氨綸%油劑
렬해기상색보질보법%안륜%유제
PY-GC/MS%spandex%filature oil
氨纶是一种聚氨酯弹性纤维,应用领域广阔。在对氨纶生产过程中产生的大量废丝进行回收重复利用时,所添加的油剂会对甬道发生堵塞,因此在氨纶废丝回收之前需要对其进行清洗来控制油剂的含量。运用裂解气相色谱-质谱法( PY-GC/MS)建立了1种测试氨纶废丝中油剂残余含量的方法。方法简单快捷,无需任何样品前处理,为氨纶废丝的清洗工作,尤其是工业化清洗生产提供了准确可靠的数据。
氨綸是一種聚氨酯彈性纖維,應用領域廣闊。在對氨綸生產過程中產生的大量廢絲進行迴收重複利用時,所添加的油劑會對甬道髮生堵塞,因此在氨綸廢絲迴收之前需要對其進行清洗來控製油劑的含量。運用裂解氣相色譜-質譜法( PY-GC/MS)建立瞭1種測試氨綸廢絲中油劑殘餘含量的方法。方法簡單快捷,無需任何樣品前處理,為氨綸廢絲的清洗工作,尤其是工業化清洗生產提供瞭準確可靠的數據。
안륜시일충취안지탄성섬유,응용영역엄활。재대안륜생산과정중산생적대량폐사진행회수중복이용시,소첨가적유제회대용도발생도새,인차재안륜폐사회수지전수요대기진행청세래공제유제적함량。운용렬해기상색보-질보법( PY-GC/MS)건립료1충측시안륜폐사중유제잔여함량적방법。방법간단쾌첩,무수임하양품전처리,위안륜폐사적청세공작,우기시공업화청세생산제공료준학가고적수거。
Spandex is a polyurethane elastic fiber known for its wide range of applications. A large amount of spandex waste is generated during the production process, which needs to be recycled. Because the filature oil of the spandex waste would block the spin system during the production process, to control the content of filature oil before the spandex waste is recycled is necessary. In this paper, a new method to determine the residual oil content in spandex waste is established using the pyrolysis gas chromatography-mass spectrometry. The method is simple, efficient, and without any sample pretreatment, the method can provide accurate and reliable residual oil data for the cleaning work of spandex waste, especially for the industrial cleaning purpose.