广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2014年
24期
46-48
,共3页
活性炭%稻壳%H3 PO4%微波%马弗炉
活性炭%稻殼%H3 PO4%微波%馬弗爐
활성탄%도각%H3 PO4%미파%마불로
activated carbon%rice husk%phosphoric acid%microwave%muffle
采用H3 PO4为活化剂、稻壳为原料,通过微波和马弗炉两种方法制备活性炭。详细考察了浸渍时间、料液比、活化剂浓度、微波功率或活化温度、以及活化时间的影响。结果显示,在磷酸浓度35％、料液质量比1：4、浸渍时间3 h的条件下,采用400 W微波功率辐射8 min,制备的活性炭亚甲基蓝吸附值达到232 mg/g,若采用马弗炉600℃焙烧10 min,活性炭的亚甲基蓝吸附值达到226 mg/g。
採用H3 PO4為活化劑、稻殼為原料,通過微波和馬弗爐兩種方法製備活性炭。詳細攷察瞭浸漬時間、料液比、活化劑濃度、微波功率或活化溫度、以及活化時間的影響。結果顯示,在燐痠濃度35％、料液質量比1：4、浸漬時間3 h的條件下,採用400 W微波功率輻射8 min,製備的活性炭亞甲基藍吸附值達到232 mg/g,若採用馬弗爐600℃焙燒10 min,活性炭的亞甲基藍吸附值達到226 mg/g。
채용H3 PO4위활화제、도각위원료,통과미파화마불로량충방법제비활성탄。상세고찰료침지시간、료액비、활화제농도、미파공솔혹활화온도、이급활화시간적영향。결과현시,재린산농도35％、료액질량비1：4、침지시간3 h적조건하,채용400 W미파공솔복사8 min,제비적활성탄아갑기람흡부치체도232 mg/g,약채용마불로600℃배소10 min,활성탄적아갑기람흡부치체도226 mg/g。
The preparation of activated carbon via microwave and muffle were introduced, taking rice husk as raw material and H3 PO4 as activating agent. Some effects on the product, such as the activation and immersion time, impregnation ratio, H3 PO4 concentration, microwave power or activation temperature were investigated. Under the optimized conditions, the methylene cyanine adsorption value of the product was 232 mg/g and 226 mg/g, respectively, when the material was radiated by microwave at 400 w for 8 min, or was calcined in muffle at 600 ℃ for 10 min.
