CAJ | 학술논문

通过对苎麻碱纤维的碱处理，以及3‐氯‐2‐羟丙基脲中间体的合成，制备并研究了新型苎麻阴离子交换功能纤维3‐脲基‐2‐羟丙基纤维素的制备工艺，并测试了苎麻阴离子交换功能纤维的主要化学成分、机械性能及其离子交换容量．对实验结果进行直观分析和方差分析，得出最优工艺参数为：中间体3‐氯‐2‐羟基丙基脲与碱纤维素的投料比为5∶1，反应时间为3h，反应温度为60℃．最后，通过扫描电镜（SEM）对产品微观形态进行观察，产物的外观形态与苎麻纤维并无太大差异．而通过红外光谱分析，可以看出光谱图上有—NH—的特征吸收峰，表明其具有阴离子交换功能基团．
통과대저마감섬유적감처리，이급3‐록‐2‐간병기뇨중간체적합성，제비병연구료신형저마음리자교환공능섬유3‐뇨기‐2‐간병기섬유소적제비공예，병측시료저마음리자교환공능섬유적주요화학성분、궤계성능급기리자교환용량．대실험결과진행직관분석화방차분석，득출최우공예삼수위：중간체3‐록‐2‐간기병기뇨여감섬유소적투료비위5∶1，반응시간위3h，반응온도위60℃．최후，통과소묘전경（SEM）대산품미관형태진행관찰，산물적외관형태여저마섬유병무태대차이．이통과홍외광보분석，가이간출광보도상유—NH—적특정흡수봉，표명기구유음리자교환공능기단．
By producing ramie alkali fibers and 3‐Ureido‐2‐Hydroxylpropyl cellulose intermediates 3‐chloro‐2‐hydroxylpropyl urea ,the ramie anion exchange functional fibers were prepared .The main chemical composition , mechanical properties and ion exchange capacity of ramie anion exchange functional fibers were measured .The optimal parameters have been obtained by the direct analysis and variance analysis ,namely reactant ratio of in‐termediates 3‐chloro‐2‐hydroxylpropyl urea is 5∶1 ,reaction time is 3 hours ,reaction temperature is 60℃ .Fi‐nally ,the microscopic observations are made through the sweeping electron microscope .There is little different appearance between anion exchange fibers and ramie fibers .The feature of absorption spectrum of —NH—group were found in infrared spectrum by infrared spectroscopy .