湖北大学学报（自然科学版）
湖北大學學報（自然科學版）
호북대학학보（자연과학판）
2015年
1期
17-20
,共4页
微波消解%ICP-AES%ABS塑料%铅
微波消解%ICP-AES%ABS塑料%鉛
미파소해%ICP-AES%ABS소료%연
microwave digestion%ICP-AES%ABS plastics%lead
建立微波消解-电感耦合等离子体原子发射光谱法测定ABS塑料中铅的含量为297.5 mg/kg.实验中消解体系为7.0 mL浓硝酸和1.5 mL30%过氧化氢，实验方法的检出限为7.35 mg/kg，精密度RSD<5%，加标回收率为88.0%~107.0%.该方法样品用量少，溶样周期短，测试速度快，适用于ABS塑料中铅含量的快速测定.
建立微波消解-電感耦閤等離子體原子髮射光譜法測定ABS塑料中鉛的含量為297.5 mg/kg.實驗中消解體繫為7.0 mL濃硝痠和1.5 mL30%過氧化氫，實驗方法的檢齣限為7.35 mg/kg，精密度RSD<5%，加標迴收率為88.0%~107.0%.該方法樣品用量少，溶樣週期短，測試速度快，適用于ABS塑料中鉛含量的快速測定.
건립미파소해-전감우합등리자체원자발사광보법측정ABS소료중연적함량위297.5 mg/kg.실험중소해체계위7.0 mL농초산화1.5 mL30%과양화경，실험방법적검출한위7.35 mg/kg，정밀도RSD<5%，가표회수솔위88.0%~107.0%.해방법양품용량소，용양주기단，측시속도쾌，괄용우ABS소료중연함량적쾌속측정.
Determination of lead in ABS plastics was studied by microwave digestion with ICP-AES.The content of lead in ABS plastics is 297.5 mg/kg. In the experiment 7.0 mL nitric acid and 1.5 mL 30%hydrogen peroxide for digesting the ABS plastics. The method limited is 7.35 mg/kg,and the recoveries rang from 88.0%to 107.0%,RSDs are less than 5%.The method is convenient and accurate,which would be used to determination of lead in ABS plastics.
