中国陶瓷工业
中國陶瓷工業
중국도자공업
CHINA CERAMIC INDUSTRY
2014年
6期
20-25
,共6页
MgO-ZrO2%复合材料%烧结%热震稳定性
MgO-ZrO2%複閤材料%燒結%熱震穩定性
MgO-ZrO2%복합재료%소결%열진은정성
MgO-ZrO2%composites%sintering%thermal shock stabilit
以烧结镁砂和单斜氧化锆粉为原料,进行了MgO-ZrO2复合材料的制备。通过XRD和SEM-EDS分析及显气孔率、体积密度、常温抗折强度、线膨胀系数和1100℃~室温水冷热震稳定性的测试,探讨了ZrO2的用量对MgO-ZrO2复合材料的烧结和热震稳定性的影响。结果表明:随着ZrO2用量的增加,复合材料试样的致密度和常温抗折强度呈现出先增大后减小的趋势,复合材料试样的热膨胀系数逐步减小,复合材料试样的热震稳定性呈现出先变好后变差的趋势;当ZrO2用量为30%时,MgO-ZrO2复合材料试样的烧结性能和热震稳定性最好。
以燒結鎂砂和單斜氧化鋯粉為原料,進行瞭MgO-ZrO2複閤材料的製備。通過XRD和SEM-EDS分析及顯氣孔率、體積密度、常溫抗摺彊度、線膨脹繫數和1100℃~室溫水冷熱震穩定性的測試,探討瞭ZrO2的用量對MgO-ZrO2複閤材料的燒結和熱震穩定性的影響。結果錶明:隨著ZrO2用量的增加,複閤材料試樣的緻密度和常溫抗摺彊度呈現齣先增大後減小的趨勢,複閤材料試樣的熱膨脹繫數逐步減小,複閤材料試樣的熱震穩定性呈現齣先變好後變差的趨勢;噹ZrO2用量為30%時,MgO-ZrO2複閤材料試樣的燒結性能和熱震穩定性最好。
이소결미사화단사양화고분위원료,진행료MgO-ZrO2복합재료적제비。통과XRD화SEM-EDS분석급현기공솔、체적밀도、상온항절강도、선팽창계수화1100℃~실온수랭열진은정성적측시,탐토료ZrO2적용량대MgO-ZrO2복합재료적소결화열진은정성적영향。결과표명:수착ZrO2용량적증가,복합재료시양적치밀도화상온항절강도정현출선증대후감소적추세,복합재료시양적열팽창계수축보감소,복합재료시양적열진은정성정현출선변호후변차적추세;당ZrO2용량위30%시,MgO-ZrO2복합재료시양적소결성능화열진은정성최호。
MgO-ZrO2 composites were prepared using magnesite clinker and monocline zirconia as raw materials. The inlfuence of ZrO2 content on the sintering and thermal shock stability of MgO-ZrO2 composites were investigated by XRD SEM-EDS and the tests of apparent porosity, bulk density, lfexural strength, linear expansibility and thermal shock stability. The results showed:with the increasing amount of ZrO2 , their density and lfexural strength at room temperature ifrst increased and then decreased, their linear expansibility reduced gradually, and their thermal shock stability ifrst rose and then lowered;MgO-ZrO2 composites showed excellent sintering performance and thermal shock stability at 30%ZrO2.