中国药师
中國藥師
중국약사
CHINA PHARMACIST
2015年
1期
154-155
,共2页
王伟影%毛菊华%余华丽%余乐%程科军
王偉影%毛菊華%餘華麗%餘樂%程科軍
왕위영%모국화%여화려%여악%정과군
柳叶蜡梅%桉油精%气相色谱法
柳葉蠟梅%桉油精%氣相色譜法
류협사매%안유정%기상색보법
Chimonanthus salicifolius S. Y. Hu%Eucalyptol%GC
目的：：建立气相色谱法测定柳叶蜡梅中桉油精含量的方法。方法：采用气相色谱法,Zebron ZB-WAX 型毛细管柱(60 m ×0.32 mm,0.5μm)；程序升温：60~200℃；氢火焰离子化检测器,检测器温度为250℃；进样口温度为220℃；高纯氮气做载气。结果：桉油精在0.0126~0.5034 mg·ml-1范围内呈良好线性关系(r=0.9998)；平均加样回收率为100.68%,RSD=1.51%(n=6)。结论：本方法简便、准确、快速、重复性好,适用于柳叶蜡梅的质量控制。
目的：：建立氣相色譜法測定柳葉蠟梅中桉油精含量的方法。方法：採用氣相色譜法,Zebron ZB-WAX 型毛細管柱(60 m ×0.32 mm,0.5μm)；程序升溫：60~200℃；氫火燄離子化檢測器,檢測器溫度為250℃；進樣口溫度為220℃；高純氮氣做載氣。結果：桉油精在0.0126~0.5034 mg·ml-1範圍內呈良好線性關繫(r=0.9998)；平均加樣迴收率為100.68%,RSD=1.51%(n=6)。結論：本方法簡便、準確、快速、重複性好,適用于柳葉蠟梅的質量控製。
목적：：건립기상색보법측정류협사매중안유정함량적방법。방법：채용기상색보법,Zebron ZB-WAX 형모세관주(60 m ×0.32 mm,0.5μm)；정서승온：60~200℃；경화염리자화검측기,검측기온도위250℃；진양구온도위220℃；고순담기주재기。결과：안유정재0.0126~0.5034 mg·ml-1범위내정량호선성관계(r=0.9998)；평균가양회수솔위100.68%,RSD=1.51%(n=6)。결론：본방법간편、준학、쾌속、중복성호,괄용우류협사매적질량공제。
Objective:To establish the quantitative method for eucalyptol in Chimonanthus salicifolius S. Y. Hu by GC. Methods:The GC method was performed on a Zebron ZB-WAX column (60 m × 0. 32 mm,0. 5 μm) with programmed temperature of 60-200℃, an FID detector was used, the detector temperature was 250℃, the inlet temperature was 220℃, and the carrier gas was nitrogen with high purity. Results:A good linearity of eucalyptol was within the range of 0. 012 6-0. 503 4 mg·ml-1(r=0. 999 8), and the average recov-ery was 100. 68%(RSD=1. 51%,n=6). Conclusion:The method is simple, accurate and quick with good reproducibility, and suitable for the quality control of Chimonanthus salicifolius S. Y. Hu.
