CAJ | 학술논문

采用HP-5毛细管柱和FID检测器，以1,2-二苯乙烷为内标物，建立气相色谱分析方法对溴丁酰草胺及杂质进行分离。该方法分离效果好，准确度高，重现性好且操作简单、快速。方法的标准偏差为0.11，变异系数为0.12%，相关系数为0.9996，平均回收率为99.47%。
채용HP-5모세관주화FID검측기，이1,2-이분을완위내표물，건립기상색보분석방법대추정선초알급잡질진행분리。해방법분리효과호，준학도고，중현성호차조작간단、쾌속。방법적표준편차위0.11，변이계수위0.12%，상관계수위0.9996，평균회수솔위99.47%。
The separation and determination method of bromobutide TC was established by GC with HP-5 column and FID detector, using diphenyl ethane as internal standard. The result indicated that the standard deviation for bromobutide was 0.11, the coefficient of variation was 0.12%, the linear correlation was 0.9996, and the average recovery was 99.47%. The method had the advantages as high efficiency, accuracy and good reproducibility.