广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2015年
4期
145-146,173
,共3页
气相色谱法%桂枝茯苓胶囊%丹皮酚
氣相色譜法%桂枝茯苓膠囊%丹皮酚
기상색보법%계지복령효낭%단피분
gas chromatography%guizhifuling capsule%paeonol
建立气相色谱法测定桂枝茯苓胶囊中丹皮酚含量的方法。色谱柱为DB-624(0.53 mm×30 m×3μm)；氢火焰离子化检测器( FID)；色谱条件：采用程序升温,110→170→230℃,升温速率10℃/min；进样口温度250℃；检测器温度300℃；流速4 mL/min；分流比11。按外标法测定丹皮酚的含量。结果表明：丹皮酚在20~200μg/mL浓度范围内与峰面积线性关系良好(r=0.9996),平均加标回收率为108.70%(RSD%=1.38, n=3)。本方法准确、可靠、快速、简便,可用于测定桂枝茯苓胶囊中丹皮酚的含量。
建立氣相色譜法測定桂枝茯苓膠囊中丹皮酚含量的方法。色譜柱為DB-624(0.53 mm×30 m×3μm)；氫火燄離子化檢測器( FID)；色譜條件：採用程序升溫,110→170→230℃,升溫速率10℃/min；進樣口溫度250℃；檢測器溫度300℃；流速4 mL/min；分流比11。按外標法測定丹皮酚的含量。結果錶明：丹皮酚在20~200μg/mL濃度範圍內與峰麵積線性關繫良好(r=0.9996),平均加標迴收率為108.70%(RSD%=1.38, n=3)。本方法準確、可靠、快速、簡便,可用于測定桂枝茯苓膠囊中丹皮酚的含量。
건립기상색보법측정계지복령효낭중단피분함량적방법。색보주위DB-624(0.53 mm×30 m×3μm)；경화염리자화검측기( FID)；색보조건：채용정서승온,110→170→230℃,승온속솔10℃/min；진양구온도250℃；검측기온도300℃；류속4 mL/min；분류비11。안외표법측정단피분적함량。결과표명：단피분재20~200μg/mL농도범위내여봉면적선성관계량호(r=0.9996),평균가표회수솔위108.70%(RSD%=1.38, n=3)。본방법준학、가고、쾌속、간편,가용우측정계지복령효낭중단피분적함량。
Aiming to establish a method for determination of paeonol in guizhifuling capsule by gas chromatography, gapillary column DB-624 (0.53 mmí30 mí3 μm) was used, and FID detector was under the following chromatography condition:column temperature was set 110 ℃→170 ℃→230 ℃, temperature rate was 10 ℃/min, injector temperature at 250 ℃ and detector at 300 ℃ respectively, velocity was 4 mL/min and split ration was 11, and xternal standards was used for quantitative determination. The results showed that there was excellent linearity between the peak area and concentration of the peaonol in the concentration range of 20 ~200 μg/mL ( r=0.9996 ) . The average recovery was 108.70% (RSD=1.38%, n=3). This method was accurate, credible, fast and easy to determine the content of paeonol in guizhifuling capsule.
