首都食品与医药
首都食品與醫藥
수도식품여의약
Capital Medicine
2015年
4期
44-45
,共2页
朱姗薇%李永利%夏晖%郑绯%潘一敏%刘峰群
硃姍薇%李永利%夏暉%鄭緋%潘一敏%劉峰群
주산미%리영리%하휘%정비%반일민%류봉군
高效液相色谱%参泽冲剂%丹参酮ⅡA
高效液相色譜%參澤遲劑%丹參酮ⅡA
고효액상색보%삼택충제%단삼동ⅡA
HPLC%Niaosaitong tablets%tanshinone IIA
目的：建立高效液相色谱测定参泽冲剂中丹参酮ⅡA含量的方法。方法采用Kromasil C18色谱柱。流动相甲醇：水(74∶26),流速1ml/min,检测波长270nm。结果丹参酮ⅡA峰与其相邻峰的分离良好，理论板数8000。对照品线性范围0.04368～0.2184μg。r=0.9999,平均回收率100.04%，RSD1.47%。结论采用高效液相色谱法测定参泽冲剂中丹参酮ⅡA含量，操作简便，结果准确。
目的：建立高效液相色譜測定參澤遲劑中丹參酮ⅡA含量的方法。方法採用Kromasil C18色譜柱。流動相甲醇：水(74∶26),流速1ml/min,檢測波長270nm。結果丹參酮ⅡA峰與其相鄰峰的分離良好，理論闆數8000。對照品線性範圍0.04368～0.2184μg。r=0.9999,平均迴收率100.04%，RSD1.47%。結論採用高效液相色譜法測定參澤遲劑中丹參酮ⅡA含量，操作簡便，結果準確。
목적：건립고효액상색보측정삼택충제중단삼동ⅡA함량적방법。방법채용Kromasil C18색보주。류동상갑순：수(74∶26),류속1ml/min,검측파장270nm。결과단삼동ⅡA봉여기상린봉적분리량호，이론판수8000。대조품선성범위0.04368～0.2184μg。r=0.9999,평균회수솔100.04%，RSD1.47%。결론채용고효액상색보법측정삼택충제중단삼동ⅡA함량，조작간편，결과준학。
Object To develop a HPLC quantitative method for the determination of tanshinone IIA in Shenze granule. Methods The chromatographic conditions include column kromacil C18 , mobile phase:methanol:water(74:26) ,flow rate of 1 ml/min and monitored at 270 nm. Results The number of theoretical plates caculated by tanshinone was 12000 , The regression equation for tanshinone IIA was Y= 5451.5x-1.6128, r=0.9999,r=0.9999,and the linear range was 0.04064μg~0.2032μg. The average recovery of tanshinone IIA was 100.04% ,RSD1.47%. Conclusion The method was sensitive, rapid and accurate for the Determination of tanshinone IIA In Niaosaitong tablets.
