CAJ | 학술논문

建立了杏仁皮中活性物质苦杏仁苷含量的测定方法，并对杏仁皮脱毒工艺进行了优化。用紫外光谱法测得：在219 nm处有最大吸收光谱；苦杏仁苷的甲醇溶液在一定的浓度范围内，其吸光度值与浓度呈良好的线性关系（r2=0.9992）。以苦杏仁苷标准品为对照，计算了样品中的苦杏仁苷含量。确定测定方法以后，对浸泡脱毒法进行单因素及正交优化，确定了0.1%柠檬酸浸泡8 h，浸泡温度70℃、料水比1∶15（g∶mL）为最佳脱毒条件。
건립료행인피중활성물질고행인감함량적측정방법，병대행인피탈독공예진행료우화。용자외광보법측득：재219 nm처유최대흡수광보；고행인감적갑순용액재일정적농도범위내，기흡광도치여농도정량호적선성관계（r2=0.9992）。이고행인감표준품위대조，계산료양품중적고행인감함량。학정측정방법이후，대침포탈독법진행단인소급정교우화，학정료0.1%저몽산침포8 h，침포온도70℃、료수비1∶15（g∶mL）위최가탈독조건。
This paper aimed to establish a method for measuring the concentration of amygdalin in almond skin. The optimization of detoxification also was finished. With Ultraviolet spectrometry , the maximum absorption wavelength determined at 219 nm , and the calibration curve was linear in a certain range(r2=0.999 2),and with the standard of amygdalin as reference, amygdalin contents in samples were measured. Based on this method, the single factors and orthogonal optimization were used for the detoxification of soaking. The result is as follows:0.1 %citric acid soaking reagent,8 hours for smoking,70℃soaking temperature,the rate of solid to liquid 1∶15(g/mL).