CAJ | 학술논문

建立高效液相色谱检测柚皮苷含量的方法，通过单因素试验考察提取时间、提取功率、乙醇体积分数和固液比4个因素对柚皮苷提取率的影响，在此基础上运用正交试验法优化柚皮苷的提取工艺。结果表明：柚皮苷的最佳提取工艺为用50%的乙醇，按固液比1∶25进行超声提取60 min，超声提取功率50 W。该优选工艺合理、稳定可行，在此优化条件下提取柚皮苷的含量是6.134%。
건립고효액상색보검측유피감함량적방법，통과단인소시험고찰제취시간、제취공솔、을순체적분수화고액비4개인소대유피감제취솔적영향，재차기출상운용정교시험법우화유피감적제취공예。결과표명：유피감적최가제취공예위용50%적을순，안고액비1∶25진행초성제취60 min，초성제취공솔50 W。해우선공예합리、은정가행，재차우화조건하제취유피감적함량시6.134%。
A high performance liquid chromatographic method was developed for determining the content of naringin.The effects of ultrasonic time, ultrasonic power,ethanol concentration and solid-liquid ratio factors on the narngin extraction rate were investigated by single-factor experiments.Based on the above work ,the extraction technology of naringin was optimized by orthogonal experiment.The optimal extraction technology was as follow:the ethanol concentration was 50%,the solid-liquid ratio was 1∶25,the ultrasonic power was 50 W and extracting time was 60 min. The extraction content of naringin was 6.134%by the above method.