CAJ | 학술논문

采用旋转摩擦挤压法制备多壁碳纳米管增强铝基(MWCNTs/Al)复合材料，通过高分辨透射电镜观察MWCNTs/Al复合材料的界面结构，并对界面反应进行研究。结果表明：在MWCNTs/Al复合材料中Al-C之间发生界面反应，两者之间的反应产物为Al4C3，其晶面间距为0.827nm，为(003)晶面；Al基体的(111)晶面与MWCNTs的(002)晶面及Al4C3的(003)晶面的界面结合良好，界面存在MWCNTs(002)∥Al4C3(003)的晶体学位相关系。
채용선전마찰제압법제비다벽탄납미관증강려기(MWCNTs/Al)복합재료，통과고분변투사전경관찰MWCNTs/Al복합재료적계면결구，병대계면반응진행연구。결과표명：재MWCNTs/Al복합재료중Al-C지간발생계면반응，량자지간적반응산물위Al4C3，기정면간거위0.827nm，위(003)정면；Al기체적(111)정면여MWCNTs적(002)정면급Al4C3적(003)정면적계면결합량호，계면존재MWCNTs(002)∥Al4C3(003)적정체학위상관계。
The multi-walled carbon nanotubes (MWCNTs) reinforced Al matrix composites were prepared by rotational friction extrusion (RFE). The interface microstructures of MWCNTs/Al composites were observed by high resolution transmission electron microscopy (HRTEM). The interface reaction was analyzed. The results show that the interface reaction occurs between the Al-C in MWCNTs/Al composites. The reaction product is Al4C3, with spaced interplanar of 0.827nm, which as (003) crystal plane of Al4C3. The interface combination among Al(111) planes, MWCNTs(002) planes and Al4C3(003) planes is well. There is crystallographic orientation relationship of MWCNTs(002) parallel to Al4C3(003) at the interface.