食品研究与开发
食品研究與開髮
식품연구여개발
FOOD RESEARCH AND CEVELOPMENT
2015年
1期
93-95,96
,共4页
雪菊%黄酮%NaNO2-Al(NO3)3-NaOH法%AlCl3法
雪菊%黃酮%NaNO2-Al(NO3)3-NaOH法%AlCl3法
설국%황동%NaNO2-Al(NO3)3-NaOH법%AlCl3법
snow chrysanthemum%flavonoids%NaNO2-Al(NO3)3-NaOH method%AlCl3 method
以芦丁为标准品，对NaNO2-Al（NO3）3-NaOH法和AlCl3法测定新疆昆仑雪菊总黄酮含量的结果作了比较。结果表明：NaNO2-Al（NO3）3-NaOH法的测定结果比AlCl3法对于高原雪菊和平原雪菊分别约高19.76 mg/mL和9.34 mg/mL， AlCl3法适宜酸度为pH>5.5。邻苯二酚干扰实验表明，平均误差为0.019 mg/L，随着邻苯二酚量的增加，测得值无上升趋势。AlCl3法的线性方程为：A=0.000638+0.8623C，r2=0.9992。因此，对含酚类、酸类较多的昆仑雪菊应采用三氯化铝法测定其总黄酮的含量。
以蘆丁為標準品，對NaNO2-Al（NO3）3-NaOH法和AlCl3法測定新疆昆崙雪菊總黃酮含量的結果作瞭比較。結果錶明：NaNO2-Al（NO3）3-NaOH法的測定結果比AlCl3法對于高原雪菊和平原雪菊分彆約高19.76 mg/mL和9.34 mg/mL， AlCl3法適宜痠度為pH>5.5。鄰苯二酚榦擾實驗錶明，平均誤差為0.019 mg/L，隨著鄰苯二酚量的增加，測得值無上升趨勢。AlCl3法的線性方程為：A=0.000638+0.8623C，r2=0.9992。因此，對含酚類、痠類較多的昆崙雪菊應採用三氯化鋁法測定其總黃酮的含量。
이호정위표준품，대NaNO2-Al（NO3）3-NaOH법화AlCl3법측정신강곤륜설국총황동함량적결과작료비교。결과표명：NaNO2-Al（NO3）3-NaOH법적측정결과비AlCl3법대우고원설국화평원설국분별약고19.76 mg/mL화9.34 mg/mL， AlCl3법괄의산도위pH>5.5。린분이분간우실험표명，평균오차위0.019 mg/L，수착린분이분량적증가，측득치무상승추세。AlCl3법적선성방정위：A=0.000638+0.8623C，r2=0.9992。인차，대함분류、산류교다적곤륜설국응채용삼록화려법측정기총황동적함량。
With rut in as the standard substance, comparing the NaNO2-Al (NO3)3-NaOH determination of total flavonoids content in Xinjiang Kunlun snow chrysanthemum method and AlCl 3 method. The results showed that:NaNO2-Al(NO3)3-NaOH assay results than the AlCl3 method for the Plateau snow chrysanthemum and plain snow chrysanthemum was approximately 19.76 mg/mL and 9.34 mg/mL, AlCl3 acidity was pH>5.5. The experiment showed that the catechol interference, the average error was 0.019 mg/L, with the increase of the measured value of catechol, no upward trend. Linear equation AlCl3 method was A=0.000 638+0.862 3C,r2=0.999 2. Therefore, determination of the total flavonoids of phenols, acids more Kunlun snow chrysanthemum should be adopted AlCl3 method.
