仪表技术与传感器
儀錶技術與傳感器
의표기술여전감기
INSTRUMENT TECHNIQUE AND SENSOR
2015年
1期
92-94
,共3页
陈萌%郭浩%杨江涛%赵苗苗%张斌珍%刘俊%薛晨阳%张文栋%唐军
陳萌%郭浩%楊江濤%趙苗苗%張斌珍%劉俊%薛晨暘%張文棟%唐軍
진맹%곽호%양강도%조묘묘%장빈진%류준%설신양%장문동%당군
微流控封装%PDMS%氧等离子体%十二烷基硫酸钠%表面改性
微流控封裝%PDMS%氧等離子體%十二烷基硫痠鈉%錶麵改性
미류공봉장%PDMS%양등리자체%십이완기류산납%표면개성
microfluidic package%PDMS%plasma%sodium dodecyl sulfate%surface modification
基于PDMS的微流控系统的键合封装技术需要PDMS表面具有良好的粘合力和亲水性,作为PDMS表面改性技术,等离子体处理工艺(Plasma)具有高效、快捷、操作简单等特点,但它存在“回复”和裂纹问题。文中介绍了一种结合Plasma和表面活性剂十二烷基硫酸钠( SDS)的二次处理工艺。先利用Plasma技术对PDMS表面进行无裂纹亲水处理,再利用十二烷基硫酸钠溶液对其表面进行二次处理。既可以避免PDMS表面出现裂纹,又可以使PDMS表面亲水性长久的保持。通过实验验证,两次处理后接触角减小为21°,表面粗糙度达到1.71 nm,且表面无裂纹,并经过键合测试后,经过二次处理的PDMS与玻璃和PDMS实现了长久的键合,验证了该工艺技术可行,为微流控系统的键合封装提供了技术基础。
基于PDMS的微流控繫統的鍵閤封裝技術需要PDMS錶麵具有良好的粘閤力和親水性,作為PDMS錶麵改性技術,等離子體處理工藝(Plasma)具有高效、快捷、操作簡單等特點,但它存在“迴複”和裂紋問題。文中介紹瞭一種結閤Plasma和錶麵活性劑十二烷基硫痠鈉( SDS)的二次處理工藝。先利用Plasma技術對PDMS錶麵進行無裂紋親水處理,再利用十二烷基硫痠鈉溶液對其錶麵進行二次處理。既可以避免PDMS錶麵齣現裂紋,又可以使PDMS錶麵親水性長久的保持。通過實驗驗證,兩次處理後接觸角減小為21°,錶麵粗糙度達到1.71 nm,且錶麵無裂紋,併經過鍵閤測試後,經過二次處理的PDMS與玻璃和PDMS實現瞭長久的鍵閤,驗證瞭該工藝技術可行,為微流控繫統的鍵閤封裝提供瞭技術基礎。
기우PDMS적미류공계통적건합봉장기술수요PDMS표면구유량호적점합력화친수성,작위PDMS표면개성기술,등리자체처리공예(Plasma)구유고효、쾌첩、조작간단등특점,단타존재“회복”화렬문문제。문중개소료일충결합Plasma화표면활성제십이완기류산납( SDS)적이차처리공예。선이용Plasma기술대PDMS표면진행무렬문친수처리,재이용십이완기류산납용액대기표면진행이차처리。기가이피면PDMS표면출현렬문,우가이사PDMS표면친수성장구적보지。통과실험험증,량차처리후접촉각감소위21°,표면조조도체도1.71 nm,차표면무렬문,병경과건합측시후,경과이차처리적PDMS여파리화PDMS실현료장구적건합,험증료해공예기술가행,위미류공계통적건합봉장제공료기술기출。
The bonding packaging technology based on polydimethylsiloxane ( PDMS) microfluidic system needs good adhe-sion and hydrophilicity in the surface of PDMS .As PDMS surface modification technology , plasma treatment process ( Plasma) has many characteristics , such as high efficiency , high speed and easy operation , but this technology has the problems of “reply” and“crack”.A secondary treatment process combined with Plasma technology and SDS was introduced in this paper .First, we made hydrophilic treatment without cracks on the PDMS surface using Plasma technology , then made secondary treatment with sodium dodecyl sulfate ( SDS) .This can not only avoid the cracks of PDMS surface , but also make the PDMS surface hydrophilic perma-nently.Through experiments, the contact angle decreases to 21 °after re-treatment, the roughness of the surface reaches to 1.71 nm, and no crack is on the surface .After bonding test , PDMS after re-treatment can bond with glass permanently , which ver-ifies the feasibility of the technology and lays the technical foundation for the bonding package of microfluidic systems .