中国油脂
中國油脂
중국유지
CHINA OILS AND FATS
2015年
1期
16-18,19
,共4页
孙明奎%胡志雄%李吉%欧阳剑%郭芳%吕艳飞%彭小磊%齐玉堂%张维农
孫明奎%鬍誌雄%李吉%歐暘劍%郭芳%呂豔飛%彭小磊%齊玉堂%張維農
손명규%호지웅%리길%구양검%곽방%려염비%팽소뢰%제옥당%장유농
米糠油%脱酸%萃取%碱炼%吸附%功能因子
米糠油%脫痠%萃取%堿煉%吸附%功能因子
미강유%탈산%췌취%감련%흡부%공능인자
rice bran oil%deacidification%extrac-tion%alkaline refining%adsorption%functional factor
以脱胶米糠油为原料,研究了醇萃取脱酸以及醇萃取脱酸后再经过碱炼或自制吸附剂吸附脱酸对米糠油中功能因子含量的影响。结果表明:甲醇和95%乙醇萃取脱酸均能较好地脱除游离脂肪酸( FFA),但从功能因子损失和米糠油得率来看,甲醇萃取脱酸效果明显好于95%乙醇,甲醇4次萃取脱酸后米糠油得率为63.95%,FFA脱除率为92.57%,谷维素、维生素E、植物甾醇的损失率分别为8.56%、32.86%、20.28%;对甲醇4次萃取脱酸后的米糠油采用质量分数为8.07%的碱液( NaOH溶液)进行碱炼脱酸时,其酸值( KOH)可降至1 mg/g以内,功能因子损失相对较少;自制吸附剂对甲醇4次萃取脱酸后的米糠油吸附脱酸可降低酸值,并且功能因子基本无损失。
以脫膠米糠油為原料,研究瞭醇萃取脫痠以及醇萃取脫痠後再經過堿煉或自製吸附劑吸附脫痠對米糠油中功能因子含量的影響。結果錶明:甲醇和95%乙醇萃取脫痠均能較好地脫除遊離脂肪痠( FFA),但從功能因子損失和米糠油得率來看,甲醇萃取脫痠效果明顯好于95%乙醇,甲醇4次萃取脫痠後米糠油得率為63.95%,FFA脫除率為92.57%,穀維素、維生素E、植物甾醇的損失率分彆為8.56%、32.86%、20.28%;對甲醇4次萃取脫痠後的米糠油採用質量分數為8.07%的堿液( NaOH溶液)進行堿煉脫痠時,其痠值( KOH)可降至1 mg/g以內,功能因子損失相對較少;自製吸附劑對甲醇4次萃取脫痠後的米糠油吸附脫痠可降低痠值,併且功能因子基本無損失。
이탈효미강유위원료,연구료순췌취탈산이급순췌취탈산후재경과감련혹자제흡부제흡부탈산대미강유중공능인자함량적영향。결과표명:갑순화95%을순췌취탈산균능교호지탈제유리지방산( FFA),단종공능인자손실화미강유득솔래간,갑순췌취탈산효과명현호우95%을순,갑순4차췌취탈산후미강유득솔위63.95%,FFA탈제솔위92.57%,곡유소、유생소E、식물치순적손실솔분별위8.56%、32.86%、20.28%;대갑순4차췌취탈산후적미강유채용질량분수위8.07%적감액( NaOH용액)진행감련탈산시,기산치( KOH)가강지1 mg/g이내,공능인자손실상대교소;자제흡부제대갑순4차췌취탈산후적미강유흡부탈산가강저산치,병차공능인자기본무손실。
Using degummed rice bran oil ( RBO) as raw material, the effects of alcohol extraction deacid-ification( AED) , alkaline refining or adsorption deacidification by self-made adsorbent after AED on the contents of functional factors in rice bran oil were investigated. The results showed that both methanol and 95% ethanol extraction deacidification could remove free fatty acids ( FFA) easily. However, from the point of the loss of functional factors and the extraction rate of rice bran oil, methanol prevailed over 95%ethanol significantly. After methanol extraction deacidification for four times, the extraction rate of rice bran oil, removal rate of FFA and the loss rates of oryzanol, vitamin E and phytosterols were 63. 95%, 92. 57%, 8. 56%, 32. 86% and 20. 28%, respectively. The acid value could be reduced within 1 mgKOH/g when 8. 07% alkaline solution was adopted in the alkaline refining after RBO methanol extrac-tion deacidification for four times, meanwhile, the functional factors could be kept well. Additionally, the self -made adsorbent could reduce the acid value of deacidified RBO by methonal extraction for four times, and there was almost no loss of functional factors.