大众科技
大衆科技
대음과기
DAZHONG KEJI
2014年
12期
65-67
,共3页
色谱%电子烟%烟碱%溶液%气化
色譜%電子煙%煙堿%溶液%氣化
색보%전자연%연감%용액%기화
Chromatography%electronic cigarette%nicotine%solution%vaporization
在电子烟烟碱液未经预处理以及经历在空气中多次蒸馏预处理两种条件下,采用热裂解气相色谱质谱(Py-GCMS)检测了电子烟烟碱液组分变化情况。未经预处理进行Py-GCMS时,由于烟碱液气化时与空气隔绝,气体组分的物质类型稳定,包含丙二醇、丙三醇和尼古丁,尼古丁含量低于10%;经历高温下空气中反复蒸馏预处理的烟碱液,气化后组分的物质类型和比例都与预处理的温度有关,蒸馏温度160℃时,尼古丁含量达到了21.07%。
在電子煙煙堿液未經預處理以及經歷在空氣中多次蒸餾預處理兩種條件下,採用熱裂解氣相色譜質譜(Py-GCMS)檢測瞭電子煙煙堿液組分變化情況。未經預處理進行Py-GCMS時,由于煙堿液氣化時與空氣隔絕,氣體組分的物質類型穩定,包含丙二醇、丙三醇和尼古丁,尼古丁含量低于10%;經歷高溫下空氣中反複蒸餾預處理的煙堿液,氣化後組分的物質類型和比例都與預處理的溫度有關,蒸餾溫度160℃時,尼古丁含量達到瞭21.07%。
재전자연연감액미경예처리이급경력재공기중다차증류예처리량충조건하,채용열렬해기상색보질보(Py-GCMS)검측료전자연연감액조분변화정황。미경예처리진행Py-GCMS시,유우연감액기화시여공기격절,기체조분적물질류형은정,포함병이순、병삼순화니고정,니고정함량저우10%;경력고온하공기중반복증류예처리적연감액,기화후조분적물질류형화비례도여예처리적온도유관,증류온도160℃시,니고정함량체도료21.07%。
Pyrolysis-Gas chromatography mass spectrometry method is used to analyze the relation between temperature and component and content of nicotine solution of electronic cigarette at two situations, namely without pretreatment on nicotine solution and after nicotine solution being evaporated five times in the air at set temperature. For the former situation, nicotine solution shows stable components, Propylene Glycol, Glycerin and nicotine, in which the content of nicotine is always lower than 10%. This is because nicotine solution is isolated from air when evaporating. For the latter situation, the component and content all change with evaporating temperature. When evaporating temperature is 160 ℃, the content of nicotine comes to 21.07%.