北华大学学报(自然科学版)
北華大學學報(自然科學版)
북화대학학보(자연과학판)
JOURNAL OF BEIHUA UNIVERSITY(NATURAL SCIENCE)
2015年
1期
118-122
,共5页
李学琴%李翔宇%亓伟%时君友%庞久寅%杜洪双
李學琴%李翔宇%亓偉%時君友%龐久寅%杜洪雙
리학금%리상우%기위%시군우%방구인%두홍쌍
杨木屑%活性炭%磷酸%硫酸
楊木屑%活性炭%燐痠%硫痠
양목설%활성탄%린산%류산
sawdust%activated carbon%phosphoric acid%sulfuric acid
以林业废弃物杨木屑为原料,采用正交试验法探讨以磷酸为主活化剂,浓硫酸为辅助活化剂,在不同工艺条件下制备活性炭,测定其亚甲基蓝脱色力和碘的吸附值,考虑活化因素对活性炭得率和吸附性能的影响,确定最佳工艺参数.试验结果表明:磷酸-硫酸活化法制备木屑活性炭的最佳工艺条件为浸渍比1∶2.5,浸渍浓度60%,活化时间90 min,活化温度550℃.
以林業廢棄物楊木屑為原料,採用正交試驗法探討以燐痠為主活化劑,濃硫痠為輔助活化劑,在不同工藝條件下製備活性炭,測定其亞甲基藍脫色力和碘的吸附值,攷慮活化因素對活性炭得率和吸附性能的影響,確定最佳工藝參數.試驗結果錶明:燐痠-硫痠活化法製備木屑活性炭的最佳工藝條件為浸漬比1∶2.5,浸漬濃度60%,活化時間90 min,活化溫度550℃.
이임업폐기물양목설위원료,채용정교시험법탐토이린산위주활화제,농류산위보조활화제,재불동공예조건하제비활성탄,측정기아갑기람탈색력화전적흡부치,고필활화인소대활성탄득솔화흡부성능적영향,학정최가공예삼수.시험결과표명:린산-류산활화법제비목설활성탄적최가공예조건위침지비1∶2.5,침지농도60%,활화시간90 min,활화온도550℃.
The various process conditions of activated carbon were prepared from waste poplar sawdust by phosphoric acid-sulfuric acid activation which used phosphoric acid as main activator and concentrated sulfuric acid as auxiliary activator according to orthogonal test. The experiment determined the methylene blue decolorizing power and iodine adsorption value of activated carbon,the influence of activating factors on the yield and adsorption properties of activated carbon was studied. The experimental results showed that the optimum process conditions of preparation of sawdust active carbon by phosphoric acid-sulfuric acid activation are impregnation ratio 1 ∶ 2. 5, impregnation concentration 60%, activation time 90 min, activation temperature 550℃.