功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2015年
4期
4016-4019
,共4页
孙华君%刘依%张勇%郭姗姗%吕来%陈文
孫華君%劉依%張勇%郭姍姍%呂來%陳文
손화군%류의%장용%곽산산%려래%진문
Bi25FeO40%水热法%纳米材料%光吸收%光电化学
Bi25FeO40%水熱法%納米材料%光吸收%光電化學
Bi25FeO40%수열법%납미재료%광흡수%광전화학
Bi2 5 FeO40%hydrothermal synthesis%nano-materials%optical absorption%photo-electrochemical property
通过水热法在钛基板上成功制备出了不同形貌的 Bi25 FeO 40纳米材料,使用 XRD 和 FE-SEM 对水热反应过程中反应的温度(160~200℃)、矿化剂的种类和浓度对产物结构及形貌的影响进行了研究,并对其生长机理进行分析。测试 Bi25 FeO 40的 UV-Vis漫反射光谱,发现其在波长400~600 nm 范围内具有良好的可见光响应;采用三电极体系测试材料的光电化学性能,结果显示纳米棒状产物对光电流的响应最快。
通過水熱法在鈦基闆上成功製備齣瞭不同形貌的 Bi25 FeO 40納米材料,使用 XRD 和 FE-SEM 對水熱反應過程中反應的溫度(160~200℃)、礦化劑的種類和濃度對產物結構及形貌的影響進行瞭研究,併對其生長機理進行分析。測試 Bi25 FeO 40的 UV-Vis漫反射光譜,髮現其在波長400~600 nm 範圍內具有良好的可見光響應;採用三電極體繫測試材料的光電化學性能,結果顯示納米棒狀產物對光電流的響應最快。
통과수열법재태기판상성공제비출료불동형모적 Bi25 FeO 40납미재료,사용 XRD 화 FE-SEM 대수열반응과정중반응적온도(160~200℃)、광화제적충류화농도대산물결구급형모적영향진행료연구,병대기생장궤리진행분석。측시 Bi25 FeO 40적 UV-Vis만반사광보,발현기재파장400~600 nm 범위내구유량호적가견광향응;채용삼전겁체계측시재료적광전화학성능,결과현시납미봉상산물대광전류적향응최쾌。
Sillenite type Bi2 5 FeO 40 has been used as the research subjects in this paper.Various Morphologies of Bi2 5 FeO 40 nano-materials have been successfully synthesized by hydrothermal method on the titanium substrate. The effect of processing parameters such as reaction temperature(1 60-200 ℃),mineralizer and stoichiometry was investigated by XRD and FE-SEM.Bi2 5 FeO 40 are found to have a good visible response ability from 400 to 600 nm through UV-Vis diffuse reflectance spectroscopy.The photo-electrochemical properties were measured by three electrodes measurements.The sample of nanorods morphology responded rapidly when irradiation.