湖南文理学院学报(自然科学版)
湖南文理學院學報(自然科學版)
호남문이학원학보(자연과학판)
JOURNAL OF HUNAN UNIVERSITY OF ARTS AND SCIENCE(SCIENCE AND TECHNOLOGY)
2015年
1期
82-85
,共4页
何君%张亮%王颖%谢涛%黄德凤
何君%張亮%王穎%謝濤%黃德鳳
하군%장량%왕영%사도%황덕봉
超高效合相色谱%卷烟烟气%滤嘴%羰基化合物
超高效閤相色譜%捲煙煙氣%濾嘴%羰基化閤物
초고효합상색보%권연연기%려취%탄기화합물
UPC2%cigarette smoke%filter%carbonyl compounds
为了研究不同滤嘴在卷烟降焦减害中的作用,提出了超高效合相色谱(UPC2)等度洗脱测定对卷烟主流烟气中8种羰基化合物的方法。研究结果表明:UPC2相对于传统的反相色谱,具有良好的正交选择性,8种羰基化合物具有良好的线性关系(R2>0.999),加标回收率为79%~93%,检出限为0.06~0.15μg/支;加入了活性炭的滤嘴对8种羰基化合物的综合过滤效果最好;滤嘴材料的选择是降低目标有害成分的关键。
為瞭研究不同濾嘴在捲煙降焦減害中的作用,提齣瞭超高效閤相色譜(UPC2)等度洗脫測定對捲煙主流煙氣中8種羰基化閤物的方法。研究結果錶明:UPC2相對于傳統的反相色譜,具有良好的正交選擇性,8種羰基化閤物具有良好的線性關繫(R2>0.999),加標迴收率為79%~93%,檢齣限為0.06~0.15μg/支;加入瞭活性炭的濾嘴對8種羰基化閤物的綜閤過濾效果最好;濾嘴材料的選擇是降低目標有害成分的關鍵。
위료연구불동려취재권연강초감해중적작용,제출료초고효합상색보(UPC2)등도세탈측정대권연주류연기중8충탄기화합물적방법。연구결과표명:UPC2상대우전통적반상색보,구유량호적정교선택성,8충탄기화합물구유량호적선성관계(R2>0.999),가표회수솔위79%~93%,검출한위0.06~0.15μg/지;가입료활성탄적려취대8충탄기화합물적종합과려효과최호;려취재료적선택시강저목표유해성분적관건。
In order to study the different filters in the effect of depressing the tar and reducing the harm, an ultra performance convergence chromatography (UPC2) is developed for analyzing eight carbonyl compounds in cigarette smoke. The results show that compared with conventional reverse-phase chromatography, this method has a good orthogonal selectivity. The eight carbonyl compounds display good linearity (R2>0.999). The standard addition recoveries range from 79%to 93%. The limits of detection of range from 0.08 to 0.05 μg/cig;The cigarette adding active carbon in filter tip has the best comprehensive filtering effect of eight carbonyl compounds; Selecting the appropriate filter material is the key to reduce the target harmful components.