稀土学报(英文版)
稀土學報(英文版)
희토학보(영문판)
JOURNAL OF RARE EARTHS
2015年
2期
202-206
,共5页
张振亚%杨睿%赵玉涛%刘满平%陈刚
張振亞%楊睿%趙玉濤%劉滿平%陳剛
장진아%양예%조옥도%류만평%진강
nanoparticles%metallic composites%sonochemistry melt reaction%microstructure%tensile properties%rare earths
In situ Al2O3np/Al-Al11Ce3 nanocomposite was successfully synthesized from Al-CeO2 system using a novel two-step processing method that combines liquid-state mechanical mixing (step-I) and sonochemistry melt reaction (step-II). The microstruc-tural evolution and mechanical properties were investigated by optical microscopy (OM), scanning electron microscopy (SEM), transmission electron spectroscopy (TEM) and tensile tests, respectively. A good spatial distribution of CeO2 particles in the Al melt was achieved due to reactive wetting during step-I, and the following formation of Al2O3np during step-II was attributed to the cavita-tion-accelerated interfacial reaction. The solidified microstructure comprised uniformly dispersed Al2O3np in the matrix and ultrafine lamellar Al-Al11Ce3 at the grain boundaries. Such unique microstructure endowed Al2O3np/Al-Al11Ce3 nanocomposite with a good balance between tensile strength (175 MPa) and ductility (18.5%). The strengthening mechanisms of the nanocomposite included grain refinement, Orowan strengthening and quench strengthening, among which Orowan strengthening contributed the most to the yield strength of the nanocomposite.