黑龙江医药
黑龍江醫藥
흑룡강의약
HEILONGJIANG MEDICAL JOURNAL
2015年
1期
63-64,65
,共3页
太成梅%金圣龙%笔雪燕%张清波
太成梅%金聖龍%筆雪燕%張清波
태성매%금골룡%필설연%장청파
高效液相色谱法%止嗽化痰胶囊%吗啡%含量测定
高效液相色譜法%止嗽化痰膠囊%嗎啡%含量測定
고효액상색보법%지수화담효낭%마배%함량측정
HPLC%Zhisouhuatan capsule%Morphine%quantitative determinatian
目的:建立止嗽化痰胶囊中吗啡含量的HPLC测定法。方法:采用TechMate C18-ST柱,流动相为乙腈-0.1%磷酸(7:93),检测波长为210nm。结果:吗啡在0.0396~0.9894μg 范围内成线性关系,平均回收率为92.8%(n=6),RSD 为1.9%。结论:本法可靠、准确,可用于该制剂的质量控制。
目的:建立止嗽化痰膠囊中嗎啡含量的HPLC測定法。方法:採用TechMate C18-ST柱,流動相為乙腈-0.1%燐痠(7:93),檢測波長為210nm。結果:嗎啡在0.0396~0.9894μg 範圍內成線性關繫,平均迴收率為92.8%(n=6),RSD 為1.9%。結論:本法可靠、準確,可用于該製劑的質量控製。
목적:건립지수화담효낭중마배함량적HPLC측정법。방법:채용TechMate C18-ST주,류동상위을정-0.1%린산(7:93),검측파장위210nm。결과:마배재0.0396~0.9894μg 범위내성선성관계,평균회수솔위92.8%(n=6),RSD 위1.9%。결론:본법가고、준학,가용우해제제적질량공제。
Objective: To establish an HPLC method of determining Morphine in Zhisouhuatan Capsule. Methods: TechMate C18-ST column was used,The mobile phase was acetonitrile-0.1%phosphoric acid (7:93) and the detection wavelength was 210nm. Results: The linear range of Germacrone was 0.0396~0.989 4μg(r=1.000 0).The average recovery was 92.8% with RSD 1.9%(n=6). Conclusion: The method is reliable,accurate and can be used to the quality control of the preparation.