矿冶工程
礦冶工程
광야공정
2014年
6期
81-84
,共4页
李荣改%宋翔宇%高志%冯艳丽%李志伟
李榮改%宋翔宇%高誌%馮豔麗%李誌偉
리영개%송상우%고지%풍염려%리지위
含锂粘土矿%焙烧%浸出%锂
含鋰粘土礦%焙燒%浸齣%鋰
함리점토광%배소%침출%리
lithium-bearing clay%roasting%leaching%Li
对河南某地低品位含锂粘土矿进行了试验研究。根据该矿石的工艺矿物学特性,采用原矿(-2 mm)焙烧?常温浸出流程,最优试验条件为:焙烧温度800℃,焙烧时间2 h,硫酸钙/原矿比0.7,氟化钙/原矿比0.2,硫酸钠/原矿比0.2,浸出时间1 h,浸出温度20℃,液固比3∶1,硫酸浓度50%,在此条件下锂浸出率为95.32%。在参考槽浸最佳条件的基础上进行了柱浸,可以获得锂浸出率为91.78%的结果。
對河南某地低品位含鋰粘土礦進行瞭試驗研究。根據該礦石的工藝礦物學特性,採用原礦(-2 mm)焙燒?常溫浸齣流程,最優試驗條件為:焙燒溫度800℃,焙燒時間2 h,硫痠鈣/原礦比0.7,氟化鈣/原礦比0.2,硫痠鈉/原礦比0.2,浸齣時間1 h,浸齣溫度20℃,液固比3∶1,硫痠濃度50%,在此條件下鋰浸齣率為95.32%。在參攷槽浸最佳條件的基礎上進行瞭柱浸,可以穫得鋰浸齣率為91.78%的結果。
대하남모지저품위함리점토광진행료시험연구。근거해광석적공예광물학특성,채용원광(-2 mm)배소?상온침출류정,최우시험조건위:배소온도800℃,배소시간2 h,류산개/원광비0.7,불화개/원광비0.2,류산납/원광비0.2,침출시간1 h,침출온도20℃,액고비3∶1,류산농도50%,재차조건하리침출솔위95.32%。재삼고조침최가조건적기출상진행료주침,가이획득리침출솔위91.78%적결과。
A low?grade lithium?bearing clay from Henan Province was taken for study. According to the mineralogical characteristics, a process of roasting followed by leaching at normal temperature was adopted in the test with the ore at size of -2 mm. Under the following optimal testing conditions:roasting at 800℃ for 2 h with calcium sulfate/ore ratio at 0.7, calcium fluoride/ore ratio at 0.2 and sodium sulfate/ore ratio at 0.2, followed by the leaching at 20℃ for 1 h with liquid?solid ratio at 3∶1, sulfuric acid concentration of 50%, the leaching rate of Li reached 95. 32%. Then a column leaching test was conducted with the best condition of tank leaching as reference, resulting in the leaching rate of Li up to 91.78%.