酿酒科技
釀酒科技
양주과기
LIQUOR-MAKING SCIENCE & TECHNOLOGY
2015年
1期
68-72
,共5页
江伟%薛洁%付方圆%王露%刘翔
江偉%薛潔%付方圓%王露%劉翔
강위%설길%부방원%왕로%류상
葡萄酒%加糖酿造%SNIF-NMR%同位素分析
葡萄酒%加糖釀造%SNIF-NMR%同位素分析
포도주%가당양조%SNIF-NMR%동위소분석
grape wine%chaptalizing%site-specific natural isotope fractionation-nuclear magnetic resonance (SNIF-NMR)%stable isotope ratio analysis
基于不同植物来源糖发酵后乙醇不同位点D/H同位素含量存在差异的原理,本研究利用点特异性天然同位素分馏核磁共振技术(SNIF-NMR)分析了加糖酿造葡萄酒乙醇分子中同位素的变化,结果表明,当添加蔗糖时,乙醇分子(D/H)Ⅰ含量上升,而R值下降;添加甜菜糖,(D/H)Ⅰ含量下降,而R值上升,乙醇(D/H)Ⅰ含量与添加的糖量呈显著正相关关系,通过测定乙醇分子中甲基位(D/H)Ⅰ的含量,可判断葡萄酒在酿造前是否进行了加糖操作。研究表明,SNIF-NMR方法是一种鉴别葡萄酒加糖种类和加糖量的有效分析技术。
基于不同植物來源糖髮酵後乙醇不同位點D/H同位素含量存在差異的原理,本研究利用點特異性天然同位素分餾覈磁共振技術(SNIF-NMR)分析瞭加糖釀造葡萄酒乙醇分子中同位素的變化,結果錶明,噹添加蔗糖時,乙醇分子(D/H)Ⅰ含量上升,而R值下降;添加甜菜糖,(D/H)Ⅰ含量下降,而R值上升,乙醇(D/H)Ⅰ含量與添加的糖量呈顯著正相關關繫,通過測定乙醇分子中甲基位(D/H)Ⅰ的含量,可判斷葡萄酒在釀造前是否進行瞭加糖操作。研究錶明,SNIF-NMR方法是一種鑒彆葡萄酒加糖種類和加糖量的有效分析技術。
기우불동식물래원당발효후을순불동위점D/H동위소함량존재차이적원리,본연구이용점특이성천연동위소분류핵자공진기술(SNIF-NMR)분석료가당양조포도주을순분자중동위소적변화,결과표명,당첨가자당시,을순분자(D/H)Ⅰ함량상승,이R치하강;첨가첨채당,(D/H)Ⅰ함량하강,이R치상승,을순(D/H)Ⅰ함량여첨가적당량정현저정상관관계,통과측정을순분자중갑기위(D/H)Ⅰ적함량,가판단포도주재양조전시부진행료가당조작。연구표명,SNIF-NMR방법시일충감별포도주가당충류화가당량적유효분석기술。
Based on the fact that the deuterium content at specific positions of alcohol molecules fermented by diverse plant source is different, in this study, SNIF-NMR was used for detecting isotope variation of alcohol molecules in chaptalizing of grape wine. The results showed that, there was significant positive correlations between the percentage of added sugar and (D/H)I isotope ratio. As cane sugar was added, (D/H)I iso-tope ratio increased and R value decreased. As beet sugar was added, (D/H)I isotope ratio decreased and R value increased. Accordingly, the use of SNIF-NMR for the detection of (D/H)I isotope ratio of alcohol molecules could judge whather chaptalizing was operated before the brewing of grape wine. SNIF-NMR is a powerful method for identifying the added sugar varieties and sugar-adding quantity for grape wine production.