广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2015年
1期
99-101
,共3页
刺头复叶耳蕨%紫外-可见吸收光谱%鉴别
刺頭複葉耳蕨%紫外-可見吸收光譜%鑒彆
자두복협이궐%자외-가견흡수광보%감별
Arachniodes exilis ching%ultraviolet-visible absorption spectrum%identification
目的：：以刺头复叶耳蕨不同萃取部位谱线组的特征为依据,较全面地反映刺头复叶耳蕨的内在品质。方法：采用紫外扫描的方式,分别对刺头复叶耳蕨石油醚(60~90℃)、乙酸乙酯、无水乙醇、水萃取部位进行扫描,得到紫外特征曲线。结果：刺头复叶耳蕨4种萃取液均在200~600 nm波长范围内有特征吸收,本测定方法的稳定性、重复性良好,4种萃取液在3 h内稳定性良好,可用于测定刺头复叶耳蕨不同萃取液在紫外-可见光区的吸收特征。结论：刺头复叶耳蕨不同极性溶剂萃取部位的紫外扫描谱线可表达其特征,为采用紫外-可见分光光度法鉴别刺头复叶耳蕨提供基础。
目的：：以刺頭複葉耳蕨不同萃取部位譜線組的特徵為依據,較全麵地反映刺頭複葉耳蕨的內在品質。方法：採用紫外掃描的方式,分彆對刺頭複葉耳蕨石油醚(60~90℃)、乙痠乙酯、無水乙醇、水萃取部位進行掃描,得到紫外特徵麯線。結果：刺頭複葉耳蕨4種萃取液均在200~600 nm波長範圍內有特徵吸收,本測定方法的穩定性、重複性良好,4種萃取液在3 h內穩定性良好,可用于測定刺頭複葉耳蕨不同萃取液在紫外-可見光區的吸收特徵。結論：刺頭複葉耳蕨不同極性溶劑萃取部位的紫外掃描譜線可錶達其特徵,為採用紫外-可見分光光度法鑒彆刺頭複葉耳蕨提供基礎。
목적：：이자두복협이궐불동췌취부위보선조적특정위의거,교전면지반영자두복협이궐적내재품질。방법：채용자외소묘적방식,분별대자두복협이궐석유미(60~90℃)、을산을지、무수을순、수췌취부위진행소묘,득도자외특정곡선。결과：자두복협이궐4충췌취액균재200~600 nm파장범위내유특정흡수,본측정방법적은정성、중복성량호,4충췌취액재3 h내은정성량호,가용우측정자두복협이궐불동췌취액재자외-가견광구적흡수특정。결론：자두복협이궐불동겁성용제췌취부위적자외소묘보선가표체기특정,위채용자외-가견분광광도법감별자두복협이궐제공기출。
To reflect intrinsic quality of Arachniodes exilis ching on the ultraviolet-visible absorption spectrum characteristics of its different extract parts. By UV scanning method, the ultraviolet-visible absorption spectrum characteristics of four different extracts including petroleum ether (60 ~90 ℃), ethyl acetate, anhydrous alumina and distilled water were determined. The four different extracts all had distinct characteristic absorption in the wavelength range of 200~600 nm, the measurement method had good reproducibility, and the four kinds of extracts had good stability within 3 h. The different extract parts of Arachniodes exilis ching was characterized by the ultraviolet-visible absorption spectrum, which can be used in the identification for quality control.
