中国兽药杂志
中國獸藥雜誌
중국수약잡지
CHINESE JOURNAL OF VETERINARY DRUG
2015年
1期
14-18
,共5页
兰新财%吴叶锋%王麦利%叶志惠%赵丽丽%姜正前
蘭新財%吳葉鋒%王麥利%葉誌惠%趙麗麗%薑正前
란신재%오협봉%왕맥리%협지혜%조려려%강정전
茯苓酸%茯苓多糖%提取工艺%正交试验
茯苓痠%茯苓多糖%提取工藝%正交試驗
복령산%복령다당%제취공예%정교시험
pachymic acid%pachyman%single factor experiment%orthogonal design
为了优化茯苓有效成分的提取工艺,分别以茯苓酸和茯苓多糖含量为考核指标,在单因素试验确定因素和水平的基础上,采用正交试验法分别对茯苓酸和茯苓多糖提取工艺进行考察。优选茯苓酸的最佳提取工艺为采用6倍药材质量的85%乙醇在55℃条件下提取1 h,优选茯苓多糖的最佳提取工艺为采用10倍药材质量的水提取3次,每次2 h。优选的提取工艺合理、稳定、可行,为进一步工业化生产提供科学的理论依据。
為瞭優化茯苓有效成分的提取工藝,分彆以茯苓痠和茯苓多糖含量為攷覈指標,在單因素試驗確定因素和水平的基礎上,採用正交試驗法分彆對茯苓痠和茯苓多糖提取工藝進行攷察。優選茯苓痠的最佳提取工藝為採用6倍藥材質量的85%乙醇在55℃條件下提取1 h,優選茯苓多糖的最佳提取工藝為採用10倍藥材質量的水提取3次,每次2 h。優選的提取工藝閤理、穩定、可行,為進一步工業化生產提供科學的理論依據。
위료우화복령유효성분적제취공예,분별이복령산화복령다당함량위고핵지표,재단인소시험학정인소화수평적기출상,채용정교시험법분별대복령산화복령다당제취공예진행고찰。우선복령산적최가제취공예위채용6배약재질량적85%을순재55℃조건하제취1 h,우선복령다당적최가제취공예위채용10배약재질량적수제취3차,매차2 h。우선적제취공예합리、은정、가행,위진일보공업화생산제공과학적이론의거。
The extraction procession of pachymic acid and pachyman from tuckahoe was optimized by single factor experiment and orthogonal design with content of pachymic acid and pachyman as the detective marker. The optimum extraction condition for pachymic acid was extracting with 6 folds of 85% alcohol at 55 ℃for 1 h under reflux. The optimum extraction condition for pachyman was extracting with 10 folds of water for 3 times, 2 h at every time. The optimized extraction condition is reasonable and scientific, and it could be used in future large-scaled preparation.