CAJ | 학술논문

目的：对市售不同产地浙贝母中有机氯农药残留和二氧化硫残留进行测定与分析，为其临床用药安全提供可靠的依据。方法采用2010年版《中国药典（一部）》中有机氯农药残留量测定法及第一增补本中二氧化硫残留量测定法，均按照2010年版《中国药典》第二增补本中限量要求进行分析。结果与结论不同产地浙江贝母中有机氯农药残留符合2010年版《中国药典》第二增补本中限度规定；二氧化硫残留根据2010年版《中国药典》第二增补本中药材及饮片鉴定通则中限度规定存在明显超标。
목적：대시수불동산지절패모중유궤록농약잔류화이양화류잔류진행측정여분석，위기림상용약안전제공가고적의거。방법채용2010년판《중국약전（일부）》중유궤록농약잔류량측정법급제일증보본중이양화류잔류량측정법，균안조2010년판《중국약전》제이증보본중한량요구진행분석。결과여결론불동산지절강패모중유궤록농약잔류부합2010년판《중국약전》제이증보본중한도규정；이양화류잔류근거2010년판《중국약전》제이증보본중약재급음편감정통칙중한도규정존재명현초표。
Objective To determine and analyze the residues of organo-chlorine pesticide and sulfur dioxide in Fritillaria thunbergii Miq. from different producing areas in domestic market to provide a reliable basis for its clinical medication safety. Methods The detection of residues of organo-chlorine pesticide adopted the method in the Chinese Pharmacopoeia(2010 edition,Volume 1),and the detection of sulfur dioxide residues adopted the method of the SupplementⅠin the Chinese Pharmacopoeia(2010 edition,Volume 1). The analysis was conducted according to the limitation requirements of the SupplementⅡ in the Chinese Pharmacopoeia(2010 edition). Results and Conclusion The residues of organo-chlorine pesticide conform to the limitation stipulation of the SupplementⅡ in the Chinese Pharmacopoeia(2010 edition),and the residues of sulfur dioxide seriously exceed the limitation stipulation of the general prin-ciples of the medicinal materials and decoction pieces verification of the Supplement Ⅱin the Chinese Pharmacopoeia(2010 edition).