中国药业
中國藥業
중국약업
CHINA PHARMACEUTICALS
2014年
24期
63-64,65
,共3页
肉豆蔻八味胶囊%总黄酮%比色法%含量测定
肉豆蔻八味膠囊%總黃酮%比色法%含量測定
육두구팔미효낭%총황동%비색법%함량측정
Roudoukou Bawei Capsules%total flavone%colorimetry%content determination
目的:对肉豆蔻八味胶囊中总黄酮的含量进行测定。方法以芦丁为对照品,用亚硝酸钠-硝酸铝-氢氧化钠显色后,在504 nm波长下测定。结果3批肉豆蔻八味胶囊中总黄酮的含量分别为21.15,20.58,20.43 mg/g,平均加样回收率为98.42%,RSD为1.13%( n=6)。结论该方法简便、准确,重复性好,可作为肉豆蔻八味胶囊的质量控制方法。
目的:對肉豆蔻八味膠囊中總黃酮的含量進行測定。方法以蘆丁為對照品,用亞硝痠鈉-硝痠鋁-氫氧化鈉顯色後,在504 nm波長下測定。結果3批肉豆蔻八味膠囊中總黃酮的含量分彆為21.15,20.58,20.43 mg/g,平均加樣迴收率為98.42%,RSD為1.13%( n=6)。結論該方法簡便、準確,重複性好,可作為肉豆蔻八味膠囊的質量控製方法。
목적:대육두구팔미효낭중총황동적함량진행측정。방법이호정위대조품,용아초산납-초산려-경양화납현색후,재504 nm파장하측정。결과3비육두구팔미효낭중총황동적함량분별위21.15,20.58,20.43 mg/g,평균가양회수솔위98.42%,RSD위1.13%( n=6)。결론해방법간편、준학,중복성호,가작위육두구팔미효낭적질량공제방법。
Objective To determine the total flavone content in Roudoukou Bawei Capsules by colorimetry. Methods With rutin as the reference substance,after coloration by sodium nitrite-aluminum nitrate-sodium hydroxide,the total flavone content in the sample was determined at the wavelength of 504 nm. Results The total flavone contents in 3 batches of of Roudoukou Bawei Capsules were 21. 15,20. 58,20. 43 mg/g respectively. The average recovery rate was 98. 42%,RSD was 1. 13%( n=6). Conclusion This method is convenient,simple and reproducible,which can be used as the quality control method of Roudoukou Bawei Capsules.