表面技术
錶麵技術
표면기술
SURFACE TECHNOLOGY
2015年
1期
102-105,111
,共5页
化学复合镀%Ni-P-PTFE%表面活性剂%摩擦磨损性能
化學複閤鍍%Ni-P-PTFE%錶麵活性劑%摩抆磨損性能
화학복합도%Ni-P-PTFE%표면활성제%마찰마손성능
electroless composite plating%Ni-P-PTFE%surfactant%friction and wear properties
目的：研究表面活性剂FC4和PTFE添加量，对Ni-P-PTFE化学复合镀层质量和镀层中PTFE体积分数的影响规律以及对镀层的摩擦磨损性能的影响。方法改变镀液中FC4和PTFE添加量，获得不同的Ni-P-PTFE化学复合镀层，用扫描电子显微镜观察镀层形貌，用能谱仪并结合直方图方法测算镀层中PTFE的体积分数，研究镀层质量和镀层中PTFE的体积分数随镀液中FC4和PTFE添加量的变化规律，测试镀层的摩擦学性能。结果 Ni-P-PTFE复合镀工艺中FC4的用量为0.3 g/L时镀层表面质量最好，镀层中PTFE体积分数最大；PTFE体积分数为10%时Ni-P-PTFE复合镀层的磨损率最小。结论镀层中PTFE的体积分数随镀液中PTFE添加量的增加而增加，对镀层磨损率的减小存在最优值。
目的：研究錶麵活性劑FC4和PTFE添加量，對Ni-P-PTFE化學複閤鍍層質量和鍍層中PTFE體積分數的影響規律以及對鍍層的摩抆磨損性能的影響。方法改變鍍液中FC4和PTFE添加量，穫得不同的Ni-P-PTFE化學複閤鍍層，用掃描電子顯微鏡觀察鍍層形貌，用能譜儀併結閤直方圖方法測算鍍層中PTFE的體積分數，研究鍍層質量和鍍層中PTFE的體積分數隨鍍液中FC4和PTFE添加量的變化規律，測試鍍層的摩抆學性能。結果 Ni-P-PTFE複閤鍍工藝中FC4的用量為0.3 g/L時鍍層錶麵質量最好，鍍層中PTFE體積分數最大；PTFE體積分數為10%時Ni-P-PTFE複閤鍍層的磨損率最小。結論鍍層中PTFE的體積分數隨鍍液中PTFE添加量的增加而增加，對鍍層磨損率的減小存在最優值。
목적：연구표면활성제FC4화PTFE첨가량，대Ni-P-PTFE화학복합도층질량화도층중PTFE체적분수적영향규률이급대도층적마찰마손성능적영향。방법개변도액중FC4화PTFE첨가량，획득불동적Ni-P-PTFE화학복합도층，용소묘전자현미경관찰도층형모，용능보의병결합직방도방법측산도층중PTFE적체적분수，연구도층질량화도층중PTFE적체적분수수도액중FC4화PTFE첨가량적변화규률，측시도층적마찰학성능。결과 Ni-P-PTFE복합도공예중FC4적용량위0.3 g/L시도층표면질량최호，도층중PTFE체적분수최대；PTFE체적분수위10%시Ni-P-PTFE복합도층적마손솔최소。결론도층중PTFE적체적분수수도액중PTFE첨가량적증가이증가，대도층마손솔적감소존재최우치。
ABSTRACT:Objective To investigate the influence rules of FC4 surfactant and PTFE addition amount on the quality of the coat-ing, the volume fraction of PTFE in the coating and the friction-wear properties. Methods Different electroless Ni-P-PTFE compos-ite platings were obtained by changing the addition amount of FC4 and PTFE. The morphology of the coatings was observed by Scanning Electron Microscope and the volume fractions of PTFE in the coatings were measured and calculated by combining Energy Disperse Spectroscopy with histogram method. The changing rules of the quality of the coatings and the volume fraction of PTFE in the coatings with the addition amount of FC4 and PTFE were investigated,and the tribological property of the coatings was analyzed. Results The best coating with the biggest volume fraction of PTFE was obtained when the addition amount of FC4 was 0. 3 g/L in the electroless Ni-P-PTFE composite plating process, and the coating with the lowest wear rate was prepared when the volume frac-tion of PTFE in the coating was 10%. Conclusion The volume fraction of PTFE in the coating increased with increasing addition a-mount of PTFE in the plating solution, and there was a minimum wear rate when the volume fraction of PTFE in the coating changed within the limit.
