中国药业
中國藥業
중국약업
CHINA PHARMACEUTICALS
2015年
8期
43-44,45
,共3页
许锋%涂瑶生%王洛临%周伟明
許鋒%塗瑤生%王洛臨%週偉明
허봉%도요생%왕락림%주위명
吴茱萸%柠檬苦素%吴茱萸碱%吴茱萸次碱%醇提工艺%正交试验
吳茱萸%檸檬苦素%吳茱萸堿%吳茱萸次堿%醇提工藝%正交試驗
오수유%저몽고소%오수유감%오수유차감%순제공예%정교시험
Euodia rutaecarpa%limonin%evodiamine%rutaecarpine%ethanol extracting process%orthogonal experiment
目的：优选吴茱萸的乙醇提取工艺。方法以柠檬苦素、吴茱萸碱和吴茱萸次碱为评价指标，采用正交试验法，对乙醇浓度、乙醇用量、提取时间和回流次数进行优选。结果吴茱萸最佳乙醇提工艺为，药材以12倍量70%乙醇回流提取2次，每次3 h。结论优选的吴茱萸醇提工艺合理可行，可为实际生产提供参考。
目的：優選吳茱萸的乙醇提取工藝。方法以檸檬苦素、吳茱萸堿和吳茱萸次堿為評價指標，採用正交試驗法，對乙醇濃度、乙醇用量、提取時間和迴流次數進行優選。結果吳茱萸最佳乙醇提工藝為，藥材以12倍量70%乙醇迴流提取2次，每次3 h。結論優選的吳茱萸醇提工藝閤理可行，可為實際生產提供參攷。
목적：우선오수유적을순제취공예。방법이저몽고소、오수유감화오수유차감위평개지표，채용정교시험법，대을순농도、을순용량、제취시간화회류차수진행우선。결과오수유최가을순제공예위，약재이12배량70%을순회류제취2차，매차3 h。결론우선적오수유순제공예합리가행，가위실제생산제공삼고。
Objective To optimize the extract process of Euodia rutaecarpa by orthogonal experiment. Methods With limonin,evodiamine and rutaecarpine as the evaluation indexes,the orthogonal experiment was adopted to optimize the ethanol concentration,ethanol amount,ex-traction time and reflux times. Results The best ethanol extraction process was that the medicinal materials were performed the reflux ex-traction with 12 times the amount of 70% ethanol,reflux extraction twice and 3 h each time. Conclusion The optimized ethanol extraction process of effective component from Euodia rutaecarpa is rational and feasible,which can provide reference for practical production.
