云南民族大学学报(自然科学版)
雲南民族大學學報(自然科學版)
운남민족대학학보(자연과학판)
JOURNAL OF YUNNAN UNIVERSITY OF THE NATIONALITIES(NATURAL SCIENCES EDITION)
2015年
2期
108-111
,共4页
孟春杨%牛德云%周斌%孟艳林%杨玉春%秦颖%胡秋芬
孟春楊%牛德雲%週斌%孟豔林%楊玉春%秦穎%鬍鞦芬
맹춘양%우덕운%주빈%맹염림%양옥춘%진영%호추분
玫瑰花%分离鉴定%苯丙素%苯乙醇
玫瑰花%分離鑒定%苯丙素%苯乙醇
매괴화%분리감정%분병소%분을순
Rosa rugosa%isolate and identify%phenylpropanoids%phenylethanoids
采用硅胶色谱、高效液相制备色谱对产自云南呈贡的玫瑰花进行分离、纯化化学成分,通过UV、IR、MS、NMR等波谱方法进行结构鉴定.分离得到了8个苯丙素和苯乙醇类已知化合物,分别鉴定为Ferulic acid(1),ω-Hydroxypropioguaiacone (2),(E)-Fenlaldehyde (3),1-Propanone-2-hydroxy-1-(3-methoxy-4-hydroxyphenyl)(4),Evofolin (5),2-(3 ′-O-p-D-Glucopyranosyl-4′-hydroxyphenyl)-ethanol (6),2-(3-Hydroxy-4-O-D-β-glucopyranosyl)phenyl-ethanol (7),2(3,4-Dihydroxy-phenyl)-ethanol(8).这些化合物均为首次从呈贡玫瑰花中分离得到.
採用硅膠色譜、高效液相製備色譜對產自雲南呈貢的玫瑰花進行分離、純化化學成分,通過UV、IR、MS、NMR等波譜方法進行結構鑒定.分離得到瞭8箇苯丙素和苯乙醇類已知化閤物,分彆鑒定為Ferulic acid(1),ω-Hydroxypropioguaiacone (2),(E)-Fenlaldehyde (3),1-Propanone-2-hydroxy-1-(3-methoxy-4-hydroxyphenyl)(4),Evofolin (5),2-(3 ′-O-p-D-Glucopyranosyl-4′-hydroxyphenyl)-ethanol (6),2-(3-Hydroxy-4-O-D-β-glucopyranosyl)phenyl-ethanol (7),2(3,4-Dihydroxy-phenyl)-ethanol(8).這些化閤物均為首次從呈貢玫瑰花中分離得到.
채용규효색보、고효액상제비색보대산자운남정공적매괴화진행분리、순화화학성분,통과UV、IR、MS、NMR등파보방법진행결구감정.분리득도료8개분병소화분을순류이지화합물,분별감정위Ferulic acid(1),ω-Hydroxypropioguaiacone (2),(E)-Fenlaldehyde (3),1-Propanone-2-hydroxy-1-(3-methoxy-4-hydroxyphenyl)(4),Evofolin (5),2-(3 ′-O-p-D-Glucopyranosyl-4′-hydroxyphenyl)-ethanol (6),2-(3-Hydroxy-4-O-D-β-glucopyranosyl)phenyl-ethanol (7),2(3,4-Dihydroxy-phenyl)-ethanol(8).저사화합물균위수차종정공매괴화중분리득도.