法医学杂志
法醫學雜誌
법의학잡지
JOURNAL OF FORENSIC MEDICINE
2015年
2期
126-128
,共3页
甘增禄%马东烈%赵春梅%刘力
甘增祿%馬東烈%趙春梅%劉力
감증록%마동렬%조춘매%류력
法医病理学%金属%铁铬合金%扫描电镜-X射线能谱仪
法醫病理學%金屬%鐵鉻閤金%掃描電鏡-X射線能譜儀
법의병이학%금속%철락합금%소묘전경-X사선능보의
forensic pathology%metals%chromiumalloys%scanning electron microscope and energy dis-persive X-ray spectrometer
目的:检测铁铬合金菜刀遗留的金属颗粒成分,并建立可行的评价指标及方法。方法使用滤纸擦蹭菜刀制作金属遗留微小颗粒样本,应用扫描电镜-X射线能谱仪(scanning electron microscopy and ener-gy dispersive X-ray spectrometer,SEM-EDX)的GSR颗粒分析功能检测遗留金属颗粒成分,计算遗留金属颗粒中铁、铬相对含量比。结果铁铬合金菜刀遗留金属颗粒内所含铁、铬相对含量比,在大部分菜刀间差异有统计学意义(P<0.05)。结论使用GSR颗粒分析功能量化检测铁铬合金菜刀遗留金属颗粒内铁、铬相对含量比,为此类致伤工具的认定建立可行的评价方法。
目的:檢測鐵鉻閤金菜刀遺留的金屬顆粒成分,併建立可行的評價指標及方法。方法使用濾紙抆蹭菜刀製作金屬遺留微小顆粒樣本,應用掃描電鏡-X射線能譜儀(scanning electron microscopy and ener-gy dispersive X-ray spectrometer,SEM-EDX)的GSR顆粒分析功能檢測遺留金屬顆粒成分,計算遺留金屬顆粒中鐵、鉻相對含量比。結果鐵鉻閤金菜刀遺留金屬顆粒內所含鐵、鉻相對含量比,在大部分菜刀間差異有統計學意義(P<0.05)。結論使用GSR顆粒分析功能量化檢測鐵鉻閤金菜刀遺留金屬顆粒內鐵、鉻相對含量比,為此類緻傷工具的認定建立可行的評價方法。
목적:검측철락합금채도유류적금속과립성분,병건립가행적평개지표급방법。방법사용려지찰층채도제작금속유류미소과립양본,응용소묘전경-X사선능보의(scanning electron microscopy and ener-gy dispersive X-ray spectrometer,SEM-EDX)적GSR과립분석공능검측유류금속과립성분,계산유류금속과립중철、락상대함량비。결과철락합금채도유류금속과립내소함철、락상대함량비,재대부분채도간차이유통계학의의(P<0.05)。결론사용GSR과립분석공능양화검측철락합금채도유류금속과립내철、락상대함량비,위차류치상공구적인정건립가행적평개방법。
Objective To establish a feasible evaluation index and method to identify composition of re-maining metal particles on ferrochrome kitchen knife. Methods The small samples of remaining metal particles were rubbed fromthe knives using filter paper. The composition of remaining metal particles was detected by scanning electron microscopy and energy dispersive X-ray spectrometer (SE m-EDX ) and GSR particle analysis function, using mathematical methods to calculate the ratio (relative amount) of Fe and Cr in remaining metal particles. Results The ratio (relative amount) of Fe and Cr of remain-ing metal particles had significant differences among most ferrochrome kitchen knives (P<0.05). Conclu-sion U sing GSR particle analysis function to quantitatively detect the ratio (relative amount) of Fe and Cr of remaining metal particles on ferrochrome kitchen knife, which can establish the feasible evaluation method to estimate such injury tool.