重庆大学学报
重慶大學學報
중경대학학보
Journal of Chongqing University (Natural Science Edition)
2015年
2期
111-117
,共7页
朱诚意%陈先红%李光强%付勇%姜玉龙
硃誠意%陳先紅%李光彊%付勇%薑玉龍
주성의%진선홍%리광강%부용%강옥룡
薄板坯连铸连轧%低温取向硅钢%第二相粒子%热轧组织
薄闆坯連鑄連軋%低溫取嚮硅鋼%第二相粒子%熱軋組織
박판배련주련알%저온취향규강%제이상입자%열알조직
compact strip production%low temperature grain-oriented silicon steel%second phase particles%hot rolled texture
研究了不同工艺生产的低温取向硅钢热轧板中第二相粒子的析出行为及其组织。结果表明,热轧板中的析出物除了弥散分布的纳米级球形或椭球形的 MnS、Cu2 S 外,还观察到与其形貌相似的 SiO2、AlN 和 Si3 N4及其复合在一起的复杂化合物。试样中微米级析出物主要为 SiO2、MnS、Cu2 S 和 AlN 的复合物,纳米级析出物主要为 AlN、Si3 N4、MnS、Cu2 S 的复合物。热轧板中0.01~0.2μm 的析出物数量最多,约占总数的99%。与常规热轧板相比,CSP 试样中夹杂物面积密度较小,在大于1μm 范围内其平均尺寸较大,会使得后期退火过程中二次再结晶不完整,影响产品磁性能。热轧板在垂直于轧向横截面上组织分布具有很大的差别,其中 CSP 试样组织相对比较均匀,不利于后续处理工艺中发展完善的二次再结晶织构从而获得良好的磁性能。
研究瞭不同工藝生產的低溫取嚮硅鋼熱軋闆中第二相粒子的析齣行為及其組織。結果錶明,熱軋闆中的析齣物除瞭瀰散分佈的納米級毬形或橢毬形的 MnS、Cu2 S 外,還觀察到與其形貌相似的 SiO2、AlN 和 Si3 N4及其複閤在一起的複雜化閤物。試樣中微米級析齣物主要為 SiO2、MnS、Cu2 S 和 AlN 的複閤物,納米級析齣物主要為 AlN、Si3 N4、MnS、Cu2 S 的複閤物。熱軋闆中0.01~0.2μm 的析齣物數量最多,約佔總數的99%。與常規熱軋闆相比,CSP 試樣中夾雜物麵積密度較小,在大于1μm 範圍內其平均呎吋較大,會使得後期退火過程中二次再結晶不完整,影響產品磁性能。熱軋闆在垂直于軋嚮橫截麵上組織分佈具有很大的差彆,其中 CSP 試樣組織相對比較均勻,不利于後續處理工藝中髮展完善的二次再結晶織構從而穫得良好的磁性能。
연구료불동공예생산적저온취향규강열알판중제이상입자적석출행위급기조직。결과표명,열알판중적석출물제료미산분포적납미급구형혹타구형적 MnS、Cu2 S 외,환관찰도여기형모상사적 SiO2、AlN 화 Si3 N4급기복합재일기적복잡화합물。시양중미미급석출물주요위 SiO2、MnS、Cu2 S 화 AlN 적복합물,납미급석출물주요위 AlN、Si3 N4、MnS、Cu2 S 적복합물。열알판중0.01~0.2μm 적석출물수량최다,약점총수적99%。여상규열알판상비,CSP 시양중협잡물면적밀도교소,재대우1μm 범위내기평균척촌교대,회사득후기퇴화과정중이차재결정불완정,영향산품자성능。열알판재수직우알향횡절면상조직분포구유흔대적차별,기중 CSP 시양조직상대비교균균,불리우후속처리공예중발전완선적이차재결정직구종이획득량호적자성능。
The precipitation behaviors of the second phase particles and their textures in the low temperature grain‐oriented silicon steel are studied under different processes.The results show that not only the dispersed nanoscale spherical or ellipsoidal MnS and Cu2 S precipitations are observed in the hot rolled slabs,but also SiO2 ,AlN and Si3 N4 which are similar to MnS and Cu2 S in the morphology and complex compounds that are composed by them together are observed.In the sample,precipitations at the micron scale are mainly composed by SiO2 ,MnS,Cu2 S and AlN,and precipitations at the nanoscale are mainly composed by AlN,Si3 N4 ,MnS and Cu2 S.The number of precipitates whose size is from 0.01 μm to 0.2 μm is the largest in the hot rolled slabs,which accounts for about 90%.Compared with the conventional hot rolling slabs,the area density of the inclusions in the CSP samples is smaller,but the average size in the range of greater than 1 μm of that is larger.It will make the secondary recrystallization incomplete during the annealing process,and also it can influence the magnetic property of the products.The distribution of texture which is perpendicular to the rolling direction on cross section in the hot rolled slabs is very different.The texture of the CSP samples is relatively uniform,which is harmful to develop complete secondary recrystallization texture during the subsequent treatment process to obtain good magnetic properties.