CAJ | 학술논문

本文采用微波法提取金莲花中黄酮，用大孔树脂对浸提液进行了提纯研究。微波法以微波时间、微波功率、固液比为三因素，设计正交试验，确定了最佳提取条件为：微波时间8min，微波功率200W，固液比1：20。提纯过程中用AB-8大孔树脂进行提纯，洗脱以乙醇浓度、乙醇用量、温度为三因素设计正交试验，确定了最佳提纯条件为：乙醇浓度75%，乙醇用量10倍，温度35℃。洗脱率可达91.6%，总黄酮纯度为51.2%。
본문채용미파법제취금연화중황동，용대공수지대침제액진행료제순연구。미파법이미파시간、미파공솔、고액비위삼인소，설계정교시험，학정료최가제취조건위：미파시간8min，미파공솔200W，고액비1：20。제순과정중용AB-8대공수지진행제순，세탈이을순농도、을순용량、온도위삼인소설계정교시험，학정료최가제순조건위：을순농도75%，을순용량10배，온도35℃。세탈솔가체91.6%，총황동순도위51.2%。
The microwave method for the extraction flavone from trollius, purification the extracting liquid by macro-reticular resin was studied in this paper. The wavelet time, wavelet power, solid-liquid tatio were regarded as three factors, by orthogonal experiment,the optimum extracting condition of lfavonoid from trollius was showed as follows:wavelet time was 8 minutes, wavelet power was 200W, solid –liquid ratio was 1:20.The AB-8 macro-reticular resin was used in purification process. The alcoholcon centration, quantity, temperature were regarded as three factors, by orthogonal experiment, the furthest purification condition was drawn as follows: alcoholcon centration was 75%, the ratio was 1:10, temperature was 35℃,thepurityoflfavonescanreachto51.2%.