药学研究
藥學研究
약학연구
JOURNAL OF PHARMACEUTICAL RESEARCH
2015年
4期
202-205
,共4页
李丹%汪冰%李晓%张中湖%巩丽萍%陆峰%褚克丹
李丹%汪冰%李曉%張中湖%鞏麗萍%陸峰%褚剋丹
리단%왕빙%리효%장중호%공려평%륙봉%저극단
表面增强拉曼光谱%银胶纸%关黄柏%非法染色%金胺O
錶麵增彊拉曼光譜%銀膠紙%關黃柏%非法染色%金胺O
표면증강랍만광보%은효지%관황백%비법염색%금알O
SERS%Ag NPs-paper%Amur Cork-tree Bark%Dyeing adulteration%Auramine O
目的:采用表面增强拉曼光谱法( SERS)对非法染色的关黄柏进行快速检测。方法采用原位还原法制备的银胶纸作为SERS基底,擦拭经乙醇溶液润湿的关黄柏,银胶纸的擦拭区立即进行SERS检测。本文先后对硝酸银的浓度、银胶纸的增强效果及稳定性等因素进行考察和优化。结果成功鉴别经0.01 mg·mL-1金胺O染料染色的关黄柏。结论表面增强拉曼光谱法可实现对染色黄药材的快速、简单、灵敏和无损的鉴别。
目的:採用錶麵增彊拉曼光譜法( SERS)對非法染色的關黃柏進行快速檢測。方法採用原位還原法製備的銀膠紙作為SERS基底,抆拭經乙醇溶液潤濕的關黃柏,銀膠紙的抆拭區立即進行SERS檢測。本文先後對硝痠銀的濃度、銀膠紙的增彊效果及穩定性等因素進行攷察和優化。結果成功鑒彆經0.01 mg·mL-1金胺O染料染色的關黃柏。結論錶麵增彊拉曼光譜法可實現對染色黃藥材的快速、簡單、靈敏和無損的鑒彆。
목적:채용표면증강랍만광보법( SERS)대비법염색적관황백진행쾌속검측。방법채용원위환원법제비적은효지작위SERS기저,찰식경을순용액윤습적관황백,은효지적찰식구립즉진행SERS검측。본문선후대초산은적농도、은효지적증강효과급은정성등인소진행고찰화우화。결과성공감별경0.01 mg·mL-1금알O염료염색적관황백。결론표면증강랍만광보법가실현대염색황약재적쾌속、간단、령민화무손적감별。
Objective To establish a surface-enhanced Raman scattering( SERS)method for the detection of dyed Amur Cork-tree Bark. Methods Supported silver nanoparticles on filter paper were synthesized by the method of in situ reduction. Experimental designs were performed to obtain the best detection results by studying the parameters:the concen-tration of silver nitrate solution,the enhancement effect and stability of the Ag NPs-paper. Results The dyed Amur Cork-tree Bark,stained by Auramine O at the concentration of 0. 01 mg·mL-1 ,had been successfully detected. Conclusion Compared with the Ag NPs-paper and SERS technology,the scheme provided a simple and rapid detection method of dyed Amur Cork-tree Bark.