CAJ | 학술논문

采用GC-MS分析油茶籽油不皂化物成分，并通过薄层层析（ TLC）对不皂化物进行初步分离。结果表明：油茶籽油不皂化物的主要成分为角鲨烯、α-生育酚，另外还有香叶基芳樟醇、麦角甾醇、β-香树脂醇、羊毛甾醇、3-乙酰菲、2，4-二叔丁基苯酚及N-（2-三氟甲基苯）-3-吡啶甲酰胺肟等物质。以石油醚与乙醚（9：1，V/V）为展开剂，通过薄层层析分离油茶籽油不皂化物，得到6条色带，利用紫外-可见光对分离物进行扫描，获得各分离物的最大吸收峰波长。
채용GC-MS분석유다자유불조화물성분，병통과박층층석（ TLC）대불조화물진행초보분리。결과표명：유다자유불조화물적주요성분위각사희、α-생육분，령외환유향협기방장순、맥각치순、β-향수지순、양모치순、3-을선비、2，4-이숙정기분분급N-（2-삼불갑기분）-3-필정갑선알우등물질。이석유미여을미（9：1，V/V）위전개제，통과박층층석분리유다자유불조화물，득도6조색대，이용자외-가견광대분리물진행소묘，획득각분리물적최대흡수봉파장。
Analyzed the unsaponifiable matters in camellia see d oil by GC-MS,and separated the unsaponifi-able matters with thin-layer chromatography( TLC). The results showed that the main components of camellia seed oil unsaponifiable matters were squalene,alpha tocopherol,geranyl linalool,ergosterol,beta amyrin,lanosterol,phe-nanthrene,3-acetyl 2,4-Di tert butyl phenol and N-(2-three trifluoromethyl benzene)-3-pyridine formamide oxime and other substances. Eluted with petroleum ether-ethyl ether(9: 1,V/V),separated the camellia seed oil unsa-ponifiables by thin layer chromatography,six bands were evidenced under ultraviolet light. Scanned the 6 isolates with UV-visible,maximum absorption peak wavelength was obtained for each isolates.