现代医药卫生
現代醫藥衛生
현대의약위생
MODERN MEDICINE HEALTH
2015年
7期
982-985
,共4页
庞学斌%张伟%邱颖姮%邬晓鸥
龐學斌%張偉%邱穎姮%鄔曉鷗
방학빈%장위%구영항%오효구
色谱法,高压液相%维生素B6%牡蛎%数学计算
色譜法,高壓液相%維生素B6%牡蠣%數學計算
색보법,고압액상%유생소B6%모려%수학계산
Chromatography,high pressure liquid%Vitamin B6%Oysters%Mathematical computing
目的:评定高效液相色谱法(HPLC法)测定牡蛎大豆肽肉碱口服液中维生素B6含量的不确定度。方法采用HPLC法测定试样中维生素B6的含量,根据建测量模型,确定影响不确定度的分量,并加以评定量化,得出合成不确定度和扩展不确定度。结果试样中维生素B6含量测得值为0.498 mg/100 mL,其中B6含量的相对不确定度为0.0249,标准不确定度为0.0124 mg/100 mL,扩展不确定度为0.0248 mg/100 mL(k=2)。结论建立的计算方法实用、可靠,可以用于HPLC法测定牡蛎大豆肽肉碱口服液中维生素B6含量的不确定度评定,经评定发现,高效液相色谱仪定量重复性对不确定度的影响最大。
目的:評定高效液相色譜法(HPLC法)測定牡蠣大豆肽肉堿口服液中維生素B6含量的不確定度。方法採用HPLC法測定試樣中維生素B6的含量,根據建測量模型,確定影響不確定度的分量,併加以評定量化,得齣閤成不確定度和擴展不確定度。結果試樣中維生素B6含量測得值為0.498 mg/100 mL,其中B6含量的相對不確定度為0.0249,標準不確定度為0.0124 mg/100 mL,擴展不確定度為0.0248 mg/100 mL(k=2)。結論建立的計算方法實用、可靠,可以用于HPLC法測定牡蠣大豆肽肉堿口服液中維生素B6含量的不確定度評定,經評定髮現,高效液相色譜儀定量重複性對不確定度的影響最大。
목적:평정고효액상색보법(HPLC법)측정모려대두태육감구복액중유생소B6함량적불학정도。방법채용HPLC법측정시양중유생소B6적함량,근거건측량모형,학정영향불학정도적분량,병가이평정양화,득출합성불학정도화확전불학정도。결과시양중유생소B6함량측득치위0.498 mg/100 mL,기중B6함량적상대불학정도위0.0249,표준불학정도위0.0124 mg/100 mL,확전불학정도위0.0248 mg/100 mL(k=2)。결론건립적계산방법실용、가고,가이용우HPLC법측정모려대두태육감구복액중유생소B6함량적불학정도평정,경평정발현,고효액상색보의정량중복성대불학정도적영향최대。
Objective Uncertainty evaluation of determination of vitamin B6 content in oyster soybean peptide carnitine oral liquid by high performance liquid chromatography(HPLC assay). Methods HPLC was adopted for the determination of vitamin B6 content. Mathematical model was established for the evaluation of uncertainty to quantize influential factors of uncertainty and evaluate the uncertainty factors further. Results The content of vitamin B6 in sample oral liquid was 0.498 mg/100mL,in which, the relative uncertaintyof vitamin B6 content was 0.024 9,the standard uncertainty was 0.0124 mg/100 mL,the expanded uncertainty was 0.024 8 mg/100 mL(k=2). Conclusion The calculation method is practical and reliable,being access to the uncertainty eval—uation of content of vitamin B6 in oyster soybean peptide carnitine oral liquid by high performance liquid chromatography. Upon the evaluation,it is found that the quantitative repetitive of the HPLC is the major impact.