内蒙古医科大学学报
內矇古醫科大學學報
내몽고의과대학학보
Journal of Inner Mongolia Medical University
2015年
1期
44-47,55
,共5页
山川柳%总黄酮%正交试验
山川柳%總黃酮%正交試驗
산천류%총황동%정교시험
ramulus tamarix%flavonoids%orthogonal test
目的::优选山川柳中总黄酮( flavonoids)的最佳提取条件。方法:以总黄酮的百分含量为指标,考察提取的温度、提取液浓度、料液比、超声时间以及提取次数等对总黄酮的百分含量的影响。又采用正交试验法,多指标分析优选山川柳中总黄酮的的提取工艺。结果:各因素对山川柳中提取总黄酮的影响次序为:提取温度>乙醇浓度>料液比>超声时间。用正交试验法得出最佳提取方案为:温度70℃,乙醇浓度60%,料液比1:30,超声40 min,提取3次。结论:该最佳提取方案得到的总黄酮百分含量高于正交试验的最高提取率,该工艺可以提高山川柳中总黄酮的提取率和纯度。
目的::優選山川柳中總黃酮( flavonoids)的最佳提取條件。方法:以總黃酮的百分含量為指標,攷察提取的溫度、提取液濃度、料液比、超聲時間以及提取次數等對總黃酮的百分含量的影響。又採用正交試驗法,多指標分析優選山川柳中總黃酮的的提取工藝。結果:各因素對山川柳中提取總黃酮的影響次序為:提取溫度>乙醇濃度>料液比>超聲時間。用正交試驗法得齣最佳提取方案為:溫度70℃,乙醇濃度60%,料液比1:30,超聲40 min,提取3次。結論:該最佳提取方案得到的總黃酮百分含量高于正交試驗的最高提取率,該工藝可以提高山川柳中總黃酮的提取率和純度。
목적::우선산천류중총황동( flavonoids)적최가제취조건。방법:이총황동적백분함량위지표,고찰제취적온도、제취액농도、료액비、초성시간이급제취차수등대총황동적백분함량적영향。우채용정교시험법,다지표분석우선산천류중총황동적적제취공예。결과:각인소대산천류중제취총황동적영향차서위:제취온도>을순농도>료액비>초성시간。용정교시험법득출최가제취방안위:온도70℃,을순농도60%,료액비1:30,초성40 min,제취3차。결론:해최가제취방안득도적총황동백분함량고우정교시험적최고제취솔,해공예가이제고산천류중총황동적제취솔화순도。
Objective:To select the optimum extracting procedure for flavonoids form Ramulus Tamarix. Methods:The yield of flavonoids was took as the index,and single-factor experiments were adopted to study the effects of extraction temperature,ultrasonic time. volume fraction of ethanol,solid to liquid ratio and extraction times on the yield of flavonoids. And orthogonal design was used to Multiple indicators analysis the extraction technology. Result:Factors affecting the yield of flavonoids ranked as extraction temperature>volume fraction of ethanol>solid to liquid ratio>ultrasonic time. Form the orthogonal the optimal processing conditions were extraction temperature,70℃,volume fraction of ethanol,60%;solid to liquid ratio,1:30(m/v,g:ml);ultrasonic time 40 min;extracting for 3 times. Conclusion:The optimal conditions was higher than any of the treatment of orthogonal test. The optimum extracting Procedure increased the content and extraction efficiency of flavonoids from Ramulus Tamarix.