菏泽学院学报
菏澤學院學報
하택학원학보
JOURNAL OF HEZE UNIVERSITY
2015年
2期
60-62
,共3页
鼻渊通窍颗粒%蒙花苷含量%野菊花%苍耳子%鉴别
鼻淵通纖顆粒%矇花苷含量%野菊花%蒼耳子%鑒彆
비연통규과립%몽화감함량%야국화%창이자%감별
Biyuantongqiao pellets%linarin%wild chrysanthemum%cocklebur%identification
对鼻渊通窍颗粒中野菊花、苍耳子的薄层鉴别及蒙花苷含量的高效液相色谱法测定进行了实验研究．结果表明，薄层色谱鉴别专属性强，斑点清晰；高效液相色谱条件下蒙花苷与其他成分能达到良好的分离，在0．045～0．615μg 范围内线性关系良好，蒙花苷回收率为101．3％．认为上述方法所得结果可靠，可用于鼻渊通窍颗粒的质量鉴定．
對鼻淵通纖顆粒中野菊花、蒼耳子的薄層鑒彆及矇花苷含量的高效液相色譜法測定進行瞭實驗研究．結果錶明，薄層色譜鑒彆專屬性彊，斑點清晰；高效液相色譜條件下矇花苷與其他成分能達到良好的分離，在0．045～0．615μg 範圍內線性關繫良好，矇花苷迴收率為101．3％．認為上述方法所得結果可靠，可用于鼻淵通纖顆粒的質量鑒定．
대비연통규과립중야국화、창이자적박층감별급몽화감함량적고효액상색보법측정진행료실험연구．결과표명，박층색보감별전속성강，반점청석；고효액상색보조건하몽화감여기타성분능체도량호적분리，재0．045～0．615μg 범위내선성관계량호，몽화감회수솔위101．3％．인위상술방법소득결과가고，가용우비연통규과립적질량감정．
An experimental study has been taken to identify wild chrysanthemum and cocklebur by TLC,and the content of linarin in pellets by HPLC.The results show that the TLC identification is specific and the spots are clear .The linarin is well -separated and the calibration curve was linear within the range of 0.045 ~0.615 μg, with the average recovery of 101 .3%.The results are reliable and can be used for quality identification of Biyuan-tongqiao pellets.
