食品研究与开发
食品研究與開髮
식품연구여개발
FOOD RESEARCH AND CEVELOPMENT
2015年
8期
85-87
,共3页
蜂蜜%微量铁%测定方法%比较
蜂蜜%微量鐵%測定方法%比較
봉밀%미량철%측정방법%비교
honey%trace iron%determination method%comparison
探讨了蜂蜜中微量铁2种测定方法。在最佳条件下采用邻二氮菲分光法测定蜂蜜试样；为保证检测结果质量，采用火焰原子吸收法对其结果进行重复检测。结果表明：采用邻二氮菲分光法和火焰原子吸收法测出某市售蜂蜜试样中铁含量分别为2.49、2.52μg/g，两者校准曲线相关性均较好，检出限分别为0.006 mg/L和0.01 mg/L，精密度RSD为0.79%和1.80%，加标回收率均在96.8%～102.7%，2种方法的测定结果无显著性差异（t=0.617，P<0.05）。
探討瞭蜂蜜中微量鐵2種測定方法。在最佳條件下採用鄰二氮菲分光法測定蜂蜜試樣；為保證檢測結果質量，採用火燄原子吸收法對其結果進行重複檢測。結果錶明：採用鄰二氮菲分光法和火燄原子吸收法測齣某市售蜂蜜試樣中鐵含量分彆為2.49、2.52μg/g，兩者校準麯線相關性均較好，檢齣限分彆為0.006 mg/L和0.01 mg/L，精密度RSD為0.79%和1.80%，加標迴收率均在96.8%～102.7%，2種方法的測定結果無顯著性差異（t=0.617，P<0.05）。
탐토료봉밀중미량철2충측정방법。재최가조건하채용린이담비분광법측정봉밀시양；위보증검측결과질량，채용화염원자흡수법대기결과진행중복검측。결과표명：채용린이담비분광법화화염원자흡수법측출모시수봉밀시양중철함량분별위2.49、2.52μg/g，량자교준곡선상관성균교호，검출한분별위0.006 mg/L화0.01 mg/L，정밀도RSD위0.79%화1.80%，가표회수솔균재96.8%～102.7%，2충방법적측정결과무현저성차이（t=0.617，P<0.05）。
The trace iron concentration in honey has been determined by phenanthroline spectrophotometry and flame atomic absorption spectrometry for quality reliability assurance. The results of two methods showed that the iron contents in honey samples were 2.49μg/g and 2.52μg/g, the correlation of calibration curve were both preferably, the detection limits were 0.006 mg/L and 0.01 mg/L, the precision RSDs were 0.79%and 1.80%, and the standardized recovery rates were 96.8%~102.7%. The results of these two methods had no significant difference by t-test (t=0. 617, P<0.05).
