西部中医药
西部中醫藥
서부중의약
GANSU JOURNAL OF TRADITIONAL CHINESE MEDICINE
2015年
4期
18-20
,共3页
姜国志%李军山%陈钟%孙胜斌
薑國誌%李軍山%陳鐘%孫勝斌
강국지%리군산%진종%손성빈
GC-MS%高良姜%配方颗粒%桉叶油醇%莰烯
GC-MS%高良薑%配方顆粒%桉葉油醇%莰烯
GC-MS%고량강%배방과립%안협유순%감희
GC-MS%galangal%formula granules%eucalyptol%camphene
目的：利用GC-MS联用技术分析高良姜配方颗粒中桉叶油醇和莰烯含量。方法：用水蒸汽蒸馏法从高良姜配方颗粒中提取挥发油，经气质分析仪分析，NIST08库定性分析桉叶油醇和莰烯，用外标法定量。结果：桉叶油醇含量0.075%，相对偏差5.4%，莰烯含量0.018%，相对偏差6.6%。结论：此方法稳定、可靠,重现性好,适用于高良姜配方颗粒中桉叶油醇和莰烯含量的分析。
目的：利用GC-MS聯用技術分析高良薑配方顆粒中桉葉油醇和莰烯含量。方法：用水蒸汽蒸餾法從高良薑配方顆粒中提取揮髮油，經氣質分析儀分析，NIST08庫定性分析桉葉油醇和莰烯，用外標法定量。結果：桉葉油醇含量0.075%，相對偏差5.4%，莰烯含量0.018%，相對偏差6.6%。結論：此方法穩定、可靠,重現性好,適用于高良薑配方顆粒中桉葉油醇和莰烯含量的分析。
목적：이용GC-MS련용기술분석고량강배방과립중안협유순화감희함량。방법：용수증기증류법종고량강배방과립중제취휘발유，경기질분석의분석，NIST08고정성분석안협유순화감희，용외표법정량。결과：안협유순함량0.075%，상대편차5.4%，감희함량0.018%，상대편차6.6%。결론：차방법은정、가고,중현성호,괄용우고량강배방과립중안협유순화감희함량적분석。
To analyze the content of eucalyptol and camphene in galangal formula granules by GC-MS. Methods: Volatile oil was extracted from galangal formula granules by steam distillation method. Qualitative analysis of eucalyptol and camphene was carried out by using GC-MS and NIST08, the mass spectra library. External standard method was adopted for quantification. Results: The content percentage of eucalyptol was 0.075% and the relative deviation was 5.4%. The percentage of the content of camphene was 0.018% and the relative deviation was 6.6%. Conclusion: This method is stable, reliable and has good reproducibility so that it is suitable for the analysis of the content of eucalyptol and camphene in galangal formula granules.
