光谱学与光谱分析
光譜學與光譜分析
광보학여광보분석
SPECTROSCOPY AND SPECTRAL ANALYSIS
2015年
4期
1001-1009
,共9页
何文绚%洪贵水%方润%蔡仙春%黄声
何文絢%洪貴水%方潤%蔡仙春%黃聲
하문현%홍귀수%방윤%채선춘%황성
植物油%筛查%红外光谱%ATR
植物油%篩查%紅外光譜%ATR
식물유%사사%홍외광보%ATR
Vegetable oil%Screen%IR%A T R
通过测定南方地区常用的花生油、玉米油、菜籽油、大豆油、葵花油、茶籽油、橄榄油等植物油以及地沟油和过期植物油的A3005(代表不饱和度)、A985(代表共轭脂肪酸含量)、A960+ A985(代表反式脂肪酸含量)三个指标值,得到了合格植物油三个指标值设定范围。在此基础上,建立快速筛查不合格植物油(过期、添加低价油、添加地沟油)的方法,有效地提高了植物油的监控效率。利用该法筛查出的若干疑不合格油,通过脂肪酸构成法和11,12,13,17脂肪酸含量判定法等,均证实它们是掺杂油或过期油,几种检测方法的结合应用,可进一步推断植物油不合格的原因。
通過測定南方地區常用的花生油、玉米油、菜籽油、大豆油、葵花油、茶籽油、橄欖油等植物油以及地溝油和過期植物油的A3005(代錶不飽和度)、A985(代錶共軛脂肪痠含量)、A960+ A985(代錶反式脂肪痠含量)三箇指標值,得到瞭閤格植物油三箇指標值設定範圍。在此基礎上,建立快速篩查不閤格植物油(過期、添加低價油、添加地溝油)的方法,有效地提高瞭植物油的鑑控效率。利用該法篩查齣的若榦疑不閤格油,通過脂肪痠構成法和11,12,13,17脂肪痠含量判定法等,均證實它們是摻雜油或過期油,幾種檢測方法的結閤應用,可進一步推斷植物油不閤格的原因。
통과측정남방지구상용적화생유、옥미유、채자유、대두유、규화유、다자유、감람유등식물유이급지구유화과기식물유적A3005(대표불포화도)、A985(대표공액지방산함량)、A960+ A985(대표반식지방산함량)삼개지표치,득도료합격식물유삼개지표치설정범위。재차기출상,건립쾌속사사불합격식물유(과기、첨가저개유、첨가지구유)적방법,유효지제고료식물유적감공효솔。이용해법사사출적약간의불합격유,통과지방산구성법화11,12,13,17지방산함량판정법등,균증실타문시참잡유혹과기유,궤충검측방법적결합응용,가진일보추단식물유불합격적원인。
In the present study ,by measuring the A3 005 (representing unsaturation) ,A985 (representing conjugated fatty acids ) , A960 + A985 (representing trans‐fatty acid ) of southern common vegetable oils (peanut oil ,corn oil ,canola oil ,soybean oil ,sun‐flower oil ,tea seed oil and olive oil) ,“waste oil”and overdue vegetable oils ,the pass‐setting‐range of these three index values for the vegetable oils was obtained .On this basis ,a method for rapid screening unqualified vegetable oil (expired ,adding low‐cost oil ,adding “waste oil”) was established .The method effectively improved the monitoring efficiency of vegetable oil .With this method of screening a number of suspected substandard oils were proved unqualified by determination of fatty acid composi‐tion and 11 ,12 ,13 ,17 fatty acid content .Through the combination of several detection methods ,the causes for disqualification of vegetable oils can be further inferred .